terclim by ICS banner
IVES 9 IVES Conference Series 9 EVALUATING WINEMAKING APPLICATIONS OF ULTRAFILTRATION TECHNOLOGY

EVALUATING WINEMAKING APPLICATIONS OF ULTRAFILTRATION TECHNOLOGY

Abstract

Ultrafiltration is a process that fractionates mixtures using semipermeable membranes, primarily on the basis of molecular weight. Depending on the nominal molecular weight cut-off (MWCO) specifications of the membrane, smaller molecules pass through the membrane into the ‘permeate’, while larger molecules are retained and concentrated in the ‘retentate’. This study investigated applications of ultrafiltra-tion technology for enhanced wine quality and profitability. The key objective was to establish to what extent ultrafiltration could be used to manage phenolic compounds (associated with astringency or bitterness) and proteins (associated with haze formation) in white wine. Nevertheless, ultrafiltration was also applied to red wine, despite the removal of anthocyanins and tannins (associated with colour and textural properties) being inherently detrimental to wine quality, so as to better characterise the chemical consequences of membrane filtration. The composition of permeate and retentate derived from pilot-scale fractionation of red and white wine using 10 and 20 kDa membranes, and different permeation rates (50, 80, 90, 95%) was investigated. The alcohol content and pH of permeate and retentate were not significantly different from that of the initial wine, but titratable acidity and macromolecules (proteins, polysaccharides and phenolic compounds, including anthocyanins for red wine) were progressively concentrated in the retentate, as a function of both membrane MWCO and the degree of permeation. Red wine permeates were stripped of much of their essential character, such that they were not considered commercially acceptable; whereas the removal of white wine phenolics demonstrated the potential for ultrafiltration to remediate oxidised or highly phenolic wines. Subsequent trials investigated the addition of retentate to (i) fermenting red grape must, (ii) dealcoholised wine, and (iii) permeate, as a potential strategies for enhancing wine colour stability, flavour intensity and/or mouthfeel properties. Whereas colour enhancements were not apparent, likely due to the inherent effects of dilution, differences in wine flavour and mouthfeel were perceived via sensory profiling using the Rate-All-That-Apply method. Findings will enable the wine industry to make informed decisions regarding the suitability of ultrafiltration technology as an innovative approach to improving wine quality and process efficiency, and therefore profitability.

DOI:

Publication date: February 9, 2024

Issue: OENO Macrowine 2023

Type: Poster

Authors

Stephanie Angela1,2, David Wollan2,3, Richard Muhlack1,2, Keren Bindon4, Kerry Wilkinson1,2

1. The University of Adelaide
2. The Australian Research Council Training Centre for Innovative Wine Production
3. VAF Memstar
4. The Australian Wine Research Institute

Contact the author*

Keywords

membranes, phenolics, proteins, wine

Tags

IVES Conference Series | oeno macrowine 2023 | oeno-macrowine

Citation

Related articles…

OPTIMIZATION OF EXTRACTION AND DEVELOPMENT OF AN LC-HRMS METHOD TO QUANTIFY GLUTATHIONE IN WHITE WINE LEES AND YEAST DERIVATIVES

Glutathione is a natural tripeptide composed of l-glutamate, l-cysteine and glycine, found in various foods and beverages. In particular, glutathione can be found in its reduced (GSH) or oxidized form (GSSG) in must, wine or yeasts¹. Numerous studies have highlighted the importance of GSH in wine quality and aging potential². During winemaking, especially during aging on lees, GSH helps prevent the harmful effects of oxidation on the aroma of the wine³. Nevertheless, the amounts of GSH/GSSG present in wine lees are often unknown and the choice of operating conditions (quantity of lees and aging time) remains empirical.

HOLISTIC APPROXIMATION OF THE INFLUENCE OF SACCHAROMYCES STRAINS ON WINE AROMA PRECURSORS

Wine varietal aroma is the result of a mixture of compounds formed or liberated from specific grape-aroma precursors. Their liberation/formation from their specific precursors can occur spontaneously by acid catalyzed rearrangements or hydrolysis or by the action of the yeast enzymatic activities. The influence of yeast during fermentation on the production of these volatile compounds has been widely studied however, the effect of this influence during aging is not fully understood. In order to evaluate these processes several indirect strategies have been used to study aroma precursors although they are not useful to understand the chemistry of the process.

WHITE WINES OXIDATIVE STABILITY: A 2-VINTAGE STUDY OF CHARDONNAY CHAMPAGNE BASE WINES AGED ON LEES IN BARRELS

Ultra-premium champagne wines are characterized by a long stay on laths. The goal of the winemaker is to use all possible oenological techniques to keep the aromatic freshness of the future products. To that purpose, some champagne base wines can be aged on lees in oak barrels. However, if it is now acknowledged that such ageing practices contribute to the oxidative stability of dry white wines, no study has been done on Chardonnay champagne base wines designed for a long ageing on laths [1].

MODELLING THE AGEING POTENTIAL OF SYRAH RED WINES BY ACCELERATED AGEING TESTS: INFLUENCE OF ANTIOXIDANT ASSAYS AND PHENOLIC COMPOSITION

Red wine ageing is an important step in the red wine evolution and impacts its chemical and sensory characteristics through many chemicals and physico-chemical reactions. The kinetics of these evolutions depend on the wine studied and influence the wine ageing potential. Generally, high quality red wines require a longer period of bottle ageing before consumption¹. The ageing potential is an impor-tant parameter for wine quality and is related to the capacity of a wine to undergo oxidation over time². Phenolic compounds which are ones of the main substrates for oxidation can then potentially modulate ageing potential³.

USING CHECK-ALL-THAT-APPLY (CATA) TO CATEGORIZE WINES: A DECISION-MAKING TOOL FOR WINE SELECTION

Bordeaux is the largest appellation vineyard in France. This contrasting vineyard with varied terroirs offers all styles of wine, resulting from the blending of several grape varieties. If these different profiles make the renown of Bordeaux wines, it can appear as a constraint when the aim is to study Bordeaux wines in their diversity. The selection of a representative sample can be performed by a sensory analysis carried out by trained panelists or by wine professionals, which can take several forms: consensus among experts, conventional descriptive analysis, typicality or quality evaluation. However, because of time, economic, and logistical constraints, these methods have limited applications. As an alternative to classical descriptive analysis, more intuitive methods that do not require training have been proposed recently to describe wines using an expert panel such as Napping, Free Choice or Flash Profiling, CATA or RATA.