terclim by ICS banner
IVES 9 IVES Conference Series 9 FOURIER TRANSFORM INFRARED SPECTROSCOPY IN MONITORING THE WINE PRODUCTION

FOURIER TRANSFORM INFRARED SPECTROSCOPY IN MONITORING THE WINE PRODUCTION

Abstract

The complexity of the wine matrix makes the monitoring of the winemaking process crucial. Fourier Transform Infrared Spectroscopy (FTIR) along with chemometrics is considered an effective analytical tool combining good accuracy, robustness, high sample throughput, and “green character”. Portable and non-portable FTIR devices are already used by the wine industry for routine analysis. However, the analytical calibrations need to be enriched, and some others are still waiting to be thoroughly developed. For this reason, an extended literature review took place identifying gaps for further research meeting the needs of the modern wine industry (Thanasi et al., 2022). The methodology that was followed was based on grouping the different studies according to the main sampling material used – 1) leaves, stems, and berries; 2) grape musts; 3) wines. For each sampling material the studies were categorized in terms of 1) main aim of the analysis; 2) type of sample; 3) sample preparation mode;4) wavenumber range (/cm); 5) spectral pre-treatment; 6) statistical method.

The most important findings were: 1) the different sample preparation modes can influence the spectra;

2) a limited number of samples (less than 100 in most cases) was used and the validation took place with cross-validation tests; 3) the developed models were not applied to different grapevine cultivars, har- vests, and types of wines; 4) many developed methods were focused on a specific oenological parameter or chemical compound or a specific stage of the winemaking process; 5) compounds with a concentration higher than 1 g/L are easier to be determined by FTIR; 6) the complexity of the wine matrix and the chemical similarity of the compounds under study makes the interpretation of the spectra very difficult due to several interferences.

1. Thanasi V., Catarino S., Ricardo-da-Silva J., 2022. Fourier-Transform Infrared Spectroscopy in monitoring the wine produc-tion. Ciência Téc. Vitiv., 37(1), 77-99. https://doi.org/10.1051/ctv/ctv2022370179

DOI:

Publication date: February 9, 2024

Issue: OENO Macrowine 2023

Type: Poster

Authors

Vasiliki Thanasi¹, Sofia Catarino1,2, Jorge Ricardo-da-Silva¹

1.LEAF – (Linking Landscape Environment Agriculture and Food ) Research Center, Instituto Superior de Agronomia, Univer-sidade de Lisboa, Tapada da Ajuda, 1349-017 Lisboa, Portugal.
2.CeFEMA – (Centre of Physics and Engineering of Advanced Materials) Research Center, Instituto Superior Técnico, Univer-sidade de Lisboa, Av. Rovisco Pais, 1, 1049-001 Lisboa, Portugal.

Contact the author*

Keywords

FTIR spectroscopy, wine, quality control, authenticity assessment

Tags

IVES Conference Series | oeno macrowine 2023 | oeno-macrowine

Citation

Related articles…

SENSORY EVALUATION OF WINE AROMA: SHOULD COLOR-DRIVEN DESCRIPTORS BE USED?

The vocabulary used to describe wine aroma is commonly organized according to color, raising the question of whether they reflect the reality of olfactory perception. Previous studies have assumed this convention of color-aroma matching, and have investigated color’s influence on the perception of aroma only in dyed white wine or in red wine from particular places of origin. Here 48 white and red varietal wines from around the world were evaluated in black glasses then in clear glasses by a panel of wine experts, who gave intensity ratings for aroma attributes commonly used by wine professionals. In black glasses, aromas conventionally associated with white wine were perceived in the red wines, and vice versa.

ACCUMULATION OF GRAPE METABOLITES IS DIFFERENTLY IMPACTED BY WATER DEFICIT AT THE BERRY AND PLANT LEVELS IN NEW FUNGUS DISEASE-TOLERANT GENOTYPES

The use of new fungus disease-tolerant varieties is a promising long-term solution to better manage chemical input in viticulture, but unfortunately little is known regarding these new hybrids fruit development and metabolites accumulation in front of abiotic stresses such as water deficit (WD). Thus, prior to the adoption of such varieties by the wine industry in Mediterranean regions, there is a need to consider their suitability to WD.

MONOSACCHARIDE COMPOSITION AND POLYSACCHARIDE FAMILIES OF LYOPHILISED EXTRACTS OBTAINED FROM POMACES OF DIFFERENT WHITE GRAPE VARIETIES

The recovery of bioactive compounds from grape and wine by-products is currently an important and necessary objective for sustainability. Grape pomace is one of the main by-products and is a rich source of some bioactive compounds such as polyphenols, polysaccharides, fatty acids, minerals and seed oil. Polysaccharides contained in the grape cell wall can be rhamnogalacturonans type II (RG-II), polysaccharides rich in arabinose and galactose (PRAG), mannoproteins (MP), homogalacturonans (HG) and non pectic polysaccharides (NPP).

EFFECT OF MANNOPROTEIN-RICH EXTRACTS FROM WINE LEES ON PHENOLICCOMPOSITION AND COLOUR OF RED WINE

In 2022, wine production was estimated at around 260 million hl. This high production rate implies to generate a large amount of by-products, which include grape pomace, grape stalks and wine lees. It is estimated that processing 100 tons of grapes leads to ~ 22 tons of by-products from which ~ 6 tons are lees [1]. Wine lees are a sludge-looking material mostly made of dead and living yeast cells, yeast debris and other particles that precipitate at the bottom of wine tanks after alcoholic fermentation. Unlike grape pomace or grape stalks, few strategies have been proposed for the recovery and valorisation of wine less [2].

EFFECTS OF WINEMAKING FACTORS AND AGEING ON THE POLYPHENOLIC AND COLORIMETRIC PROFILES IN RED WINES PRONE TO COLOUR INSTABILITY

The effects of (A) grape freezing, and (B) malolactic fermentation, have been evaluated on the chemical and colorimetric profiles of red wines from Schiava grossa cv. grapes, thus prone to colour instability. The aim was to observe if specific variables (e.g. grape freezing) could improve the extraction and stability of pigments. The samples were studied from musts up to twelve months in bottle. The study was conducted with independent parallel micro-vinifications (12 = 4 theses x 3 replicates) under strictly-controlled conditions.