terclim by ICS banner
IVES 9 IVES Conference Series 9 FOURIER TRANSFORM INFRARED SPECTROSCOPY IN MONITORING THE WINE PRODUCTION

FOURIER TRANSFORM INFRARED SPECTROSCOPY IN MONITORING THE WINE PRODUCTION

Abstract

The complexity of the wine matrix makes the monitoring of the winemaking process crucial. Fourier Transform Infrared Spectroscopy (FTIR) along with chemometrics is considered an effective analytical tool combining good accuracy, robustness, high sample throughput, and “green character”. Portable and non-portable FTIR devices are already used by the wine industry for routine analysis. However, the analytical calibrations need to be enriched, and some others are still waiting to be thoroughly developed. For this reason, an extended literature review took place identifying gaps for further research meeting the needs of the modern wine industry (Thanasi et al., 2022). The methodology that was followed was based on grouping the different studies according to the main sampling material used – 1) leaves, stems, and berries; 2) grape musts; 3) wines. For each sampling material the studies were categorized in terms of 1) main aim of the analysis; 2) type of sample; 3) sample preparation mode;4) wavenumber range (/cm); 5) spectral pre-treatment; 6) statistical method.

The most important findings were: 1) the different sample preparation modes can influence the spectra;

2) a limited number of samples (less than 100 in most cases) was used and the validation took place with cross-validation tests; 3) the developed models were not applied to different grapevine cultivars, har- vests, and types of wines; 4) many developed methods were focused on a specific oenological parameter or chemical compound or a specific stage of the winemaking process; 5) compounds with a concentration higher than 1 g/L are easier to be determined by FTIR; 6) the complexity of the wine matrix and the chemical similarity of the compounds under study makes the interpretation of the spectra very difficult due to several interferences.

1. Thanasi V., Catarino S., Ricardo-da-Silva J., 2022. Fourier-Transform Infrared Spectroscopy in monitoring the wine produc-tion. Ciência Téc. Vitiv., 37(1), 77-99. https://doi.org/10.1051/ctv/ctv2022370179

DOI:

Publication date: February 9, 2024

Issue: OENO Macrowine 2023

Type: Poster

Authors

Vasiliki Thanasi¹, Sofia Catarino1,2, Jorge Ricardo-da-Silva¹

1.LEAF – (Linking Landscape Environment Agriculture and Food ) Research Center, Instituto Superior de Agronomia, Univer-sidade de Lisboa, Tapada da Ajuda, 1349-017 Lisboa, Portugal.
2.CeFEMA – (Centre of Physics and Engineering of Advanced Materials) Research Center, Instituto Superior Técnico, Univer-sidade de Lisboa, Av. Rovisco Pais, 1, 1049-001 Lisboa, Portugal.

Contact the author*

Keywords

FTIR spectroscopy, wine, quality control, authenticity assessment

Tags

IVES Conference Series | oeno macrowine 2023 | oeno-macrowine

Citation

Related articles…

EVOLUTION OF CHEMICAL AND SENSORIAL PROFILE OF WINES ELABORATED WITH THEIR OWN TOASTED VINE-SHOOTS AND MICRO-OXYGENATION

The positive contribution of toasted vine-shoots (SEGs, Shoot from vines – Enological – Granule) used in winemaking to the chemical and sensory profile of wines has been widely proven. However, the combination of this new enological tool with other winemaking technologies, such as micro-oxygenation (MOX), has not been studied so far. It is known that micro-oxygenation is used in wineries to stabilizes color, improves structure or combining with oak alternatives products to achieve a more effective aroma integration of wines. For that, its implementation in combination with SEGs could result in differentiated wines.

EXPLORING THE INFLUENCE OF S. CEREVISIAE MANNOPROTEINS ON WINE ASTRINGENCY AND THE IMPACT OF THEIR POLYSACCHARIDE STRUCTURE

Mannoproteins (MPs) are proteoglycans from the outmost layer of yeast cell walls released into wine during alcoholic fermentation and ageing on lees processes. The use of commercial preparations of mannoproteins as additives to improve wine stability with regards to the crystallization of tartaric salts and to prevent protein haze in the case of white and rosé wines is authorized by the OIV.
Regarding red wines and polyphenols, mannoproteins are described as able to improve their colloidal stability and modulate the astringent effect of condensed tannins. The latter interact with salivary proteins forming insoluble aggregates that cause a loss of lubrication in the mouth and promote a drying and puckering sensation. However, neither the interaction mechanisms involved in mannoproteins capacity to impact astringency nor the structure-function relationships related to this property are fully understood.

ANTI-TRANSPIRANT MODULATION OF GRAPE RIPENING: EFFECTS ON MERLOT VINE DEVELOPMENT AND ROSÉ WINE PHENOLIC AND AROMATIC PROFILES

Climate changes are impacting viticultural regions throughout the world with temperature increases being most prevalent.1 These changes will not only impact the regions capable of growing grapes, but also
the grapes that can be grown.2 As temperatures rise the growing degree days increase and with it the sugar accumulation within the berries and subsequent alcohol levels in wine. Consequently, viticultural
practices need to be examined to decrease the levels of sugars.

ANTHOCYANINS EXTRACTION FROM GRAPE POMACE USING EUTECTIC SOLVENTS

Grape pomace is one of the main by-products generated after pressing in winemaking.Emerging methods, such as ultrasound-assisted extraction with eutectic mixtures, have great potential due to their low toxicity, and high biodegradability. Choline chloride (ChCl) was used as a hydrogen bond acceptor and its corresponding hydrogen bond donor (malic acid, citric acid, and glycerol: urea). Components were heated at 80 °C and stirred until a clear liquid was obtained. Distilled water was added (30 % v/v). A solid-liquid ratio of 1 g pomace per 10 ml of eutectic solvent was used.

SENSORY CHARACTERIZATION OF COGNAC EAUX-DE-VIE AGED IN BARRELS REPRESENTING DIFFERENT TOASTING PROCESS

Cognac is an outstanding french wine spirit appreciated around the world and produced exclusively in the Nouvelle-Aquitaine region, and more precisely in the Cognac area. According to AOC regulations (Appellation D’origine Controlée), the spirit required at least 2 years of continuous ageing in oak barrels to be granted the title of Cognac. The oak wood will import color, structure and organoleptic complexity. The different steps during barrel-making process, such as seasoning and toasting, influence the above quality attributes in both wines and spirits.