terclim by ICS banner
IVES 9 IVES Conference Series 9 EVALUATING WINEMAKING APPLICATIONS OF ULTRAFILTRATION TECHNOLOGY

EVALUATING WINEMAKING APPLICATIONS OF ULTRAFILTRATION TECHNOLOGY

Abstract

Ultrafiltration is a process that fractionates mixtures using semipermeable membranes, primarily on the basis of molecular weight. Depending on the nominal molecular weight cut-off (MWCO) specifications of the membrane, smaller molecules pass through the membrane into the ‘permeate’, while larger molecules are retained and concentrated in the ‘retentate’. This study investigated applications of ultrafiltra-tion technology for enhanced wine quality and profitability. The key objective was to establish to what extent ultrafiltration could be used to manage phenolic compounds (associated with astringency or bitterness) and proteins (associated with haze formation) in white wine. Nevertheless, ultrafiltration was also applied to red wine, despite the removal of anthocyanins and tannins (associated with colour and textural properties) being inherently detrimental to wine quality, so as to better characterise the chemical consequences of membrane filtration. The composition of permeate and retentate derived from pilot-scale fractionation of red and white wine using 10 and 20 kDa membranes, and different permeation rates (50, 80, 90, 95%) was investigated. The alcohol content and pH of permeate and retentate were not significantly different from that of the initial wine, but titratable acidity and macromolecules (proteins, polysaccharides and phenolic compounds, including anthocyanins for red wine) were progressively concentrated in the retentate, as a function of both membrane MWCO and the degree of permeation. Red wine permeates were stripped of much of their essential character, such that they were not considered commercially acceptable; whereas the removal of white wine phenolics demonstrated the potential for ultrafiltration to remediate oxidised or highly phenolic wines. Subsequent trials investigated the addition of retentate to (i) fermenting red grape must, (ii) dealcoholised wine, and (iii) permeate, as a potential strategies for enhancing wine colour stability, flavour intensity and/or mouthfeel properties. Whereas colour enhancements were not apparent, likely due to the inherent effects of dilution, differences in wine flavour and mouthfeel were perceived via sensory profiling using the Rate-All-That-Apply method. Findings will enable the wine industry to make informed decisions regarding the suitability of ultrafiltration technology as an innovative approach to improving wine quality and process efficiency, and therefore profitability.

DOI:

Publication date: February 9, 2024

Issue: OENO Macrowine 2023

Type: Poster

Authors

Stephanie Angela1,2, David Wollan2,3, Richard Muhlack1,2, Keren Bindon4, Kerry Wilkinson1,2

1. The University of Adelaide
2. The Australian Research Council Training Centre for Innovative Wine Production
3. VAF Memstar
4. The Australian Wine Research Institute

Contact the author*

Keywords

membranes, phenolics, proteins, wine

Tags

IVES Conference Series | oeno macrowine 2023 | oeno-macrowine

Citation

Related articles…

IDENTIFICATION AND LEVELS OF PHENOLIC COMPOUNDS (TANINS, ANTHO-CYANS) IN RED VARIETAL WINES (PROKUPAC AND BLACK TAMJANIKA) FROM SERBIA

The phenolic compounds of red wines represent a source of numerous benefits for human health, which is why they are a constant subject of scientific research. Winemaking in Serbia has a growing economic significance, with particularly autochthonous varieties included [1]. This research identifies and quantifies phenolic compounds of Serbian red varietal wines of Prokupac and Black Tamjanika varieties. Quantification of the level of phenolics has been conducted, including molecular tannins [(+)-catechin, (-)-epicatechin, procyanidin dimers B1, B2, B3, B4], molecular anthocyanins, and the mean degree of polymerization of tannins by HPLC by UV detection, total antioxidant capacity via spectrophotometric methods and chromatic characteristics via CIELAB.

OPTIMIZING THE IDENTIFICATION OF NEW THIOLS AT TRACE LEVEL IN AGED RED WINES USING NEW OAK WOOD FUNCTIONALISATION STRATEGY

During bottle aging, many thiol compounds are involved in the expression of bouquet of great aged red wines according to the quality of the closure.1,2 Identifying thiol compounds in red wines is a challenging task due several drawbacks including, the complexity of the matrix, the low concentration of these impact compounds and the amount of wine needed.3,4
This work aims to develop a new strategy based on the functionalisation of oak wood organic extracts with H₂S, to produce new thiols, in order to mimic what can happen in red wine during bottle aging. Following this approach and through sensory analysis experiments, we demonstrated that the vanilla-like aroma of fresh oak wood was transformed into intense “meaty” nuances similar to those found in old but non oxidized red wines.

PESTICIDE RESIDUES IN THE VINEYARD ENVIRONMENTS: VINE LEAVES, GRAPE BERRIES, WINES, HONEYBEES AND ASIAN HORNETS

Synthetic pesticides are widely used in viticulture to ensure steady harvest quality and quantity. Fungicides are primarily used to control grapevine diseases but insecticides and herbicides are likewise used. Pesticide residues in viticultural areas currently represent a strong societal concern, but may also affect different trophic chains in such areas. In this project we wish to analyse honeybees collected from hives placed in different vineyards, their natural predator (the invasive hornet Vespa velutina), as well as the honey, grape berries, and wines produced.

IMPACT OF NEW BIO STIMULANTS ON GRAPE SECONDARY METABOLITES UNDER CLIMATE CHANGE CONDITIONS

In a context of climate change and excessive use of agrochemical products, sustainable approaches for environmental and human health such as the use of bio stimulants in viticulture represent a potential option, against abiotic and biotic threats. Bio stimulants are organic compounds, microbes, or a combination of both, that stimulate plant’s vital processes, allowing high yields and good quality products. In vines, may trigger an innate immune response leading to the synthesis of secondary metabolites, key compounds for the organoleptic properties of grapes and wines.

YEAST LEES OBTAINED AFTER STARMERELLA BACILLARIS FERMENTATION AS A SOURCE OF POTENTIAL COMPOUNDS TO IMPROVE SUSTAINABILITY IN WINE- MAKING

The yeast residue left over after wine-making, known as wine yeast lees, is a source of various compounds that are of interest for wine and food industry. In winemaking, yeast-derived glycocompounds and proteins represent an example of circular economy approach since they have been proven to reduce the need for bentonite and animal-based fining agents. This leads to a reduced environmental impact in the stabilization and fining processes in winemaking. (de Iseppi et al., 2020, 2021).