Macrowine 2021
IVES 9 IVES Conference Series 9 Bentonite fining in cold wines: prediction tests, reduced efficiency and possibilities to avoid additional fining treatments

Bentonite fining in cold wines: prediction tests, reduced efficiency and possibilities to avoid additional fining treatments

Abstract

Bentonite fining is widely used to prevent protein haze in white wines. Most wineries use laboratory-scale fining trials to define the appropriate amount of bentonite to be used in the cellar. Those pre-tests need to mimic as much as possible the industrial scale fining procedure to determine the exact amount of bentonite necessary for protein stability. Nevertheless it is frequent that, after fining with the recommended amount of bentonite, wines appear still unstable and need an additional fining treatment. It remains a major challenge to understand why the same wine, fined with the same dosage of the same bentonite, achieves stability in the lab, but not in the cellar. Presently unclear is the role, wine temperature plays in this issue. The impact of wine temperature, pH and mixing, on the fining efficiency of different bentonites has been studied in a Gewürztraminer wine. Three different types of bentonites were used in this trial; a sodium-bentonite, a sodium-calcium-bentonite and a sodium-calcium-bentonite which additionally contains tannins. This paper shows the effects of low wine temperatures on the efficiency of three different commercial bentonites. Further, the effect of an additional whirling up of the settled bentonite is studied to understand if this could be a measure to increase the effectiveness of the fining treatment. Wine temperature has an impact on the performance of the bentonite fining. Low temperatures make it more difficult to achieve protein stability for all the different bentonites in investigation. Not one single wine achieved protein stability when it was fined at 4°C with any of the three bentonites in investigation. At low wine temperature always an additional fining treatment or anew shaking of the wines was necessary to achieve protein stability. Especially the sodium-bentonite Bentogran showed an important loss in efficiency when wines were cold. NaCalit and Super Black Jell were less affected from low wine temperatures and achieved tolerable turbidity levels when bentonite was stirred up again after one week of contact. Mixing up the settled bentonite once again when settled is an efficient way to improve the effectiveness of the bentonite fining. This simple and easy to carry out measure can be an interesting strategy for the praxis to avoid additional fining treatments. Further, to reduce the discrepancy among the laboratory and cellar conditions, two possibilities exist: (a) fining trials could be conducted at the same temperature as the wine in the cellar has, (b) bentonite fining in the cellar should not occur at too low wine temperatures. These are relevant findings for winemakers who do their bentonite fining in cold wines and deal with varieties with a high wine pH.

Publication date: May 17, 2024

Issue: Macrowine 2016

Type: Poster

Authors

Konrad Pixner*, Andreas Putti, Norbert Kofler

*Laimburg

Contact the author

Tags

IVES Conference Series | Macrowine | Macrowine 2016

Citation

Related articles…

Effect of malolactic fermentation in barrels or stainless steel tanks on wine composition. Influence of the barrel toasting

Ellagitannin, anthocyanin and woody volatile composition of Cabernet Sauvignon wines aged in oak barrels for 12 months was evaluated. Depending on the container where malolactic fermentation (MLF) was carried out, two wine modalities were investigated: wines with MLF carried out in stainless steel tanks and barrel-fermented wines. Three toasting methods (medium toast, MT; medium toast with watering, MTAA; noisette) were considered for ageing of each wine modality. Sensory analyses (triangle and rating tests) were also performed. Two-way ANOVA of the raw experimental data revealed that the toasting method and the container where MLF took place, as well as the interaction between both factors, have a significant influence (p < 0.05) on ellagitannin, anthocyanin and woody volatile profiles of Cabernet Sauvignon wines.

The impact of branched chain and aromatic amino acids on fermentation kinetics and aroma biosynthesis by wine yeast Saccharomyces cerevisiae

One of the major determinants of wine quality is the aroma. Wine aroma is the human perception of the matrix of grape and yeast derived volatiles and their interaction that contribute to flavour wine. Most common are higher alcohols, ester and aldehydes. In previous studies the formation of characteristic volatile compounds have been linked to the metabolism of branched-chain and aromatic amino acids
(BCAAs) in synthetic grape must. Here we report on an investigation to assess the impact of the initial amino acid concentration on the production of aroma compounds by the industrial yeast VIN13 grown in both synthetic and real grape musts.

Attractiveness and sweetness of red wines: Synergies between American oak barrels and mannoproteins

In partnership with a Bordeaux property wanting to improve the quality of its second wine, the effects of two factors, American oak barrels and mannoproteins were studied. Their impact on the attractiveness and sweetness of wines were characterized during two successive vintages (2012 and 2013). Vinification took place with a homogeneous batch of Cabernet Sauvignon. The wine was then divided up into various groups of five barrels of French and American oak, new or reused. Analyses of volatile and non-volatile wood compounds were undertaken at four months and eight months of wood ageing, by LC-MS and GC-MS.

Extraction of polyphenols from grape marc by supercritical fluid extraction (SFE) and evaluation of their ‘bioavailability’ as dietary supplements

In the winemaking process, several compounds that remain in the grape skins and seeds after the fermentation stage are bioactive-compounds (substances with potential beneficial effects on health) that can be extracted in order to recovery valuable substances with a high commercial value for the cosmetic, food (nutraceuticals) and pharmaceutical industries. The skins contain significant amounts of bioactive substances such as tannins (16-27%) and other polyphenolic compounds (2-6.5%) in particular, catechins, anthocyanins, proanthocyanins, quercetin , ellagic acid and resveratrol.

Novel analytical technologies for wine fingerprinting in and beyond the laboratory

For characterization, sensory designing and authentication rapid analytical technologies have become available. Some, like Proton Transfer Reaction Mass Spectrometry allow a rapid spectrum of the volatile compounds of wines. Combined with chemometrics wines can be characterized. The same approach can be used to calculate the results of virtual mixtures and allow formulation of constant quality blends. Other new techniques and portable devices based on spectroscopy allow measurements on production sites and in grocery stores, even for the smart consumer. We will present some examples of the application of these techniques for authentication of wines, both in the laboratory and on site.