Macrowine 2021
IVES 9 IVES Conference Series 9 Evidence for terroir effect associated with botrytisation relatively to compounds implicated in typical aromas of noble rot sweet wines

Evidence for terroir effect associated with botrytisation relatively to compounds implicated in typical aromas of noble rot sweet wines

Abstract

Recent studies have demonstrated the role of certain lactones, particularly 2-nonen-4-olide, and volatile thiols (3-sulfanylhexan-1-ol) in the over ripped aromas of noble rot sweet wines (Stamatopoulos et al. 2014ab). These compounds are partly formed during the maturation and under the activity of B. cinerea on grapes. This research was carried out in the vineyard of Sauternes with aim to better understand their genesis depending on the grape over-ripening on two different soil types during 3 vintages. Thus, the study was conducted, with the Sémillon grape, during vintages 2012, 2014 & 2015, at 4 stages of over-maturation of the grapes (healthy, pourri plein, pourri roti, pourri roti + 15 days) considering two vineyard plots with different soil characteristics (calcosol & peyrosol) planted with the 315 Sémillon clone and grafted on 101-14 rootstock respectively in 1981 and 1980 and cultivated with the same vineyard management. Volatile lactones were assayed by liquid-liquid extraction followed by GC/MS analysis and the precursors of 3-sulfanylhexanol by an adaptation of the method by Capone et al. 2010 (SPE-UPLC/FTMS). All the analyses were performed in grape juice. In agreement with Miklosy & Kerényi (2004) and Sarrazin (2007), the quantification of lactone compounds has confirmed the important role of B. cinerea in increasing their content during the over-ripening of the grapes. However, our observations indicated an evolution that is not similar and depends on the molecular structure of lactones. While the concentrations of saturated lactones i.e. γ-nonalactone continued to increase in the last stage (pourri roti + 15 days), the contents of unsaturated lactones i.e. 2-nonen-4-olide and massoia lactone reached their maximum at the “pourri roti” stage. Moreover, this study also showed differences in the concentration of lactones between the different vintages (2012, 2014 & 2015) and between the vineyards plots, with always higher content for both saturated and unsaturated lactones on the peyrosol plot. Given the sensory impact of 2-nonen-4-olide and massoia lactone, these could be considered as molecular markers for the quality of the noble rot sweet wines. Concerning the quantification of the 3-sulfanylhexan-1-ol precursors, the results showed differences depending on the vintage, the stage of B. cinerea maturation and the vineyard plot. First, depending on the stage of noble rot development, increasing content of precursors is associated with the impact of B. cinerea as previously observed by Thibon et al. (2009). Regarding the vintage, higher levels of S-conjugates precursors were observed in 2014 in comparison with 2012 vintage. Finally, as for lactones, the level of S-conjugates precursors seems to be dependent on the nature of soil, with differences between the vineyards plots and higher content on the peyrosol plot. Keywords: B. cinerea, sweet wines, lactones, S-conjugates aroma precursors, aroma.

Publication date: May 17, 2024

Issue: Macrowine 2016

Type: Article

Authors

Panagiotis Stamatopoulos*, Cécile Thibon, Philippe Darriet, Francis Mayeur, Sandrine Garbay

*Université de Bordeaux, ISVV

Contact the author

Tags

IVES Conference Series | Macrowine | Macrowine 2016

Citation

Related articles…

Development of a new sustainable filtering media for wine and beer clarification and sterilisation

Different separation techniques are frequently used during vinification process. Nowadays, clarification and microbiological stabilization of wine or beer can be done using precoat filters or crossflow filters to remove yeast and bacteria. Kieselguhr powders are the most used filter aids for precoat filtration. Their crystalline structure and their pulverulent nature induce ecotoxicological risks when used. Moreover, regeneration and reuse of these filter aids is not efficient and the filtration waste requires cost effective retreatment.

Towards multi-purpose valorisation of polyphenols from grape pomace: Pressurized liquid extraction coupled to purification by membrane processes

Grape by-products (including skins, seeds, stems and vine shoots) are rich in health promoting polyphenols. Their extraction from winery waste and their following purification are of special interest to produce extracts with high added value compounds. Meanwhile, the growing concern over environmental problems associated with economic constraints, require the development of environmentally sustainable extraction technologies. The extraction using semi-continuous subcritical water, as a natural solvent at high temperature and high pressure a technology is promising “green” technology that is environmentally friendly, energy efficient and improve the extraction process in plant tissues.

Correlations between sensory characteristics and colloidal content in dry white wines

Must clarification is an important step occurring just after grape extraction in the elaboration of white wine, consisting in a solid-liquid separation. Traditionally, low must turbidity, around 50-150 NTU, is generally reached in white winemaking in order to prevent reductive aromas and facilitating alcoholic fermentation. Alternatively, a higher turbidity (300 NTU or above) can be sought for reasons such as a better expression of grapes identity (terroir), or for getting a must matrix that could supposedly lead to wines having greater ageing potential.

Sensory impacts of the obturator used for the Chasselas: study over the time

Many parameters affect the organoleptic characteristics of wine: internal parameters like the chemical composition or polyphenol content and external as for example storage conditions or the type of obturator. The aim of this study was to characterize sensorally the impacts of several type of obturator on a white wine: Chasselas. To determine the organoleptic characteristics of this wine, a quantitative descriptive analysis could be used. But rapid sensory methods were preferred in this project. Indeed these methods are an appropriate alternative to conventional descriptive methods for quickly assessing sensory product discrimination.

Impact of heating must before fermentation on Chardonnay wines

Prefermentation steps of white winemaking are very important for controlling the stability and the sensory attributes of wines. Usually musts are clarified by cold settling to prevent the start of the fermentation, before racking big lees and thus limiting the appearance of vegetable or reduction off flavour while favouring an aromatic expression with low turbidity. Besides, to reach the protein stability, some white wines further require a bentonite fining, sometimes associated with negative effects on the sensory quality. This study aims to know the impact of musts heating after pressing on a Chardonnay wine in northern conditions by comparison with a classic cold racking of the must.