IVAS 2022 banner
IVES 9 IVES Conference Series 9 IVAS 9 IVAS 2022 9 Combined high-resolution chromatography techniques and sensory analysis as a support decision system tool for the oenologist

Combined high-resolution chromatography techniques and sensory analysis as a support decision system tool for the oenologist

Abstract

One of the main challenges in the wine industry is to understand how different wine processing techniques and practices can influence the overall quality of the final product. Winemakers base the decision process mostly on their personal experience, which is often influenced by emotional aspects not always scientifically supported. Other issues come from the terroir and climate change, which are affecting the quality and production techniques, both in vineyards and wineries. In addition, it is important to consider that wine culture in the different production areas is also extremely variegated, even within the same country. Relying on analytical methods is a necessary step taken in many parts of the winemaking process, starting from the determination of the optimal time for the harvest. Monitoring the fermentation is usually performed by controlling the density or the residual sugars: secondary metabolites are usually not determined. This means that in some cases the fermentation can get stuck without really knowing the reason.

This research project aims to create a predictive multivariate statistical tool in order to support the winemaker during the workflow in the winery. So, the oenologist can obtain the desired style of wine by extracting information from correlating basic oenological parameters with high resolution and sensory analysis.

Pinot Noir cultivar is a very important variety for South Tyrol representing 9.1% of the local vineyard (source: vinialtoadige.com). The experimental scheme shown in figure 1 was developed in collaboration with a South Tyrolean winery. The study plan was aimed at ensuring control over the winemaking protocols while still working at the winery production scale (90 hL per experiment).

The experimental plan included four vineyards. Besides, for one of these vineyards, the plan included the study of a viticultural technique (treatment of the canopy with chitosan prior to harvest), and two different oenological treatments: pre fermentative 4-days cryo-maceration and 7-days grape freezing. The samples were analyzed by HS-SPME-GCxGC-ToF/MS for volatile compounds, HPLC-DAD-FLD for phenolic compounds with off-line HPLC-MS/MS to identify the components, and sensory analysis by quantitative descriptive analysis (QDA®) (Poggesi, et al., 2021). The study was repeated in two different vintages (2019 and 2020) with three replicates.

As a result, multivariate statistic models showed good separations between vineyards, frozen grapes, and the cryo-macerated treatment, and separation between chitosan treatment and the control treatment. Furthermore, the time evolution of the main chemical markers was evaluated. Finally, the results obtained on the 2019 vintage were supported by the 2020 ones

References

Alto Adige Wine – Exquisite Wines from Northern Italy (altoadigewines.com)
Poggesi, S., de Matos, A. D., Longo, E., Chiotti, D., Pedri, U., Eisenstecken, D., Robatscher, P., & Boselli, E. (2021). Chemosensory profile of South Tyrolean pinot blanc wines: A multivariate regression approach. Molecules, 26(20), 1–18. https://doi.org/10.3390/molecules26206245

DOI:

Publication date: June 23, 2022

Issue: IVAS 2022

Type: Article

Authors

Poggesi Simone¹, Darnal¹, Merkyte¹, Longo¹, Montali²and Boselli ¹

¹Faculty of Science and Technology, Free University of Bozen-Bolzano
²Faculty of Computer Science, Free University of Bozen-Bolzano

Contact the author

Keywords

Pinot Noir, bidimensional gas chromatography, non-volatile phenols, support decision tool, sensory analysis

Tags

IVAS 2022 | IVES Conference Series

Citation

Related articles…

Impact of climate change on the viticultural climate of the Protected Designation of Origin “Jumilla” (SE Spain)

Protected Designation of Origin “Jumilla” (PDO Jumilla) is located in the Spanish provinces of Albacete and Murcia, in the South-eastern part of the Iberian Peninsula, where most of the models predict a severe impact of climate change in next decades. PDO Jumilla covers an area of 247,054 hectares, of which more than 22,000 hectares

Influence of weather and climatic conditions on the viticultural production in Croatia

The research includes an analysis of the impact of weather conditions on phenological development of the vine and grape quality, through monitoring of four experimental cultivars (Chardonnay, Graševina, Merlot and Plavac mali) over two production years. In each experimental vineyard, which were evenly distributed throughout the regions of Slavonia and The Croatian Danube, Croatian Uplands,

Combining effect of leaf removal and natural shading on grape ripening under two irrigation strategies in Manto negro (Vitis vinifera L.)

The increasingly frequent heat waves during grape ripening pose challenges for high quality wine grape production. Defoliation is a common practice that can improve the control of diseases in bunches, but also it increases the exposure to sunlight. Grapes exposed to solar radiation reach temperatures over the optimum for berry development and maturation. This makes the development of irrigation and canopy management techniques of great importance to maximize yield and grape quality. A field experiment was carried out during 2021 using Manto negro wine grapes to study the effect of applied irrigation and different light exposure levels on grape quality. Two irrigation treatments were imposed based on the frequency and amount of water doses in a four-block experimental vineyard at Bodega Ribas (Mallorca). Three light exposure treatments were randomly applied in each irrigation plot. The light treatments included exposed clusters from pea size, non-exposed clusters, and shaded clusters after softening. Leaf area index and canopy porosity was estimated every 2 weeks. Midday leaf water potential was measured weekly. Additionally, apparent electrical conductivity was measured between rows to estimate the soil water content variability. Light and temperature sensors were installed at the bunch level to quantify the differences in bunch temperature and light intensity among treatments. The effect of irrigation and cluster light exposure on berry weight, TSS, TA, malic acid, tartaric acid, K+, and pH were analysed at 5 moments along grape ripening. During different heat waves, the natural shading technique decreased the maximum bunch temperature around 10 °C respect to the exposed bunches in both irrigation strategies. The combination of defoliation and shading techniques after softening decreased TSS at harvest and affected most of the quality parameters during the last stages of ripening, showing an interesting technique to delay ripening in warm viticulture areas.

Current climate change in the Oplenac wine-growing district (Serbia)

Serbian autochthonous vine varieties Smederevka (for white wines) and Prokupac (for rosé and red wines) are the primary representatives of typical characteristics of wines and terroir of numerous wine-growing areas in Serbia. In the past, these varieties were the leading vine varieties, however, as the result of globalization of winemaking and the trend of consumption of wines from widely prevalent vine varieties, they were replaced by introduced international varieties. Smederevka and Prokupac vine varieties are characterized by later time of grape ripening, and relative sensitivity to low temperatures. Climate conditions can be a restrictive factor for production of high-quality grapes and wine and for the spatial spreading of these varieties in hilly continental wine-growing areas.
This paper focuses on the spatial analysis of changes of main climate parameters, in particular, analysis of viticultural bioclimatic indices that were determined for the purposes of viticulture zoning of wine-growing areas in the period 1961-2010, and those same parameters determined for the current, that is, referential climate period (1988-2017). Results of the research, that is, analysis of climate changes indicate that the majority of examined climate parameters in the Oplenac wine-growing district improved from the perspective of Smederevka and Prokupac vine varieties. These studies of climate conditions indicate that changes of analyzed climate parameters, that is, bioclimatic indices will be favorable for cultivation of varieties with later grape ripening times and those more sensitive to low temperatures, such as the autochthonous vine varieties Smederevka and Prokupac, therefore, it is recommended to producers to more actively plant vineyards with these varieties in the territory of the Oplenac wine-growing district.

Effect of partial net shading on the temperature and radiation in the grapevine canopy, consequences on the grape quality of cv. Gros Manseng in PDO Pacherenc-du-vic-Bilh

As elsewhere, southwestern France vineyards face more recurrent summer heat waves these last years. Among the possibilities of adaptation to this climate changing parameter, the use of net shading is a technique that allow for limiting canopy exposure to radiations. In this trial, we tested net shading installed on one face of the canopy, on a north-south row-oriented plot of cv. Gros Manseng trained on VSP system in the PDO Pacherenc-du-Vic-Bilh. The purpose was to characterize the effects on the ambient canopy temperatures and radiations during the season and to observe the consequences on the composition of grapes and wines. Two sorts of net were used with two levels of obstruction (50% and 75%) of the photosynthesis active radiation (PAR). They have been installed on the west side of the canopy and compared to a netless control. Temperature and PAR sensors registered hourly data during the season. On specific summer day (hot and sunny) manual measurements took also place on bunches (temperature) and in different spots of the canopy (PAR). The results showed that, on clear days, the radiation is lowered by the shade nets respecting the supplier criteria. The effects on the ambient canopy temperature were inconstant on this plot when we observed the data from the global period of shading between fruit set and harvest. However, during hot days (>30°C), the temperature in the canopy was reduced during afternoon and the temperature of the bunch surface was reduced as well comparing to the control. A decrease of the maturity parameters of the berries, sugar and acidity, was also observed. Concerning the wine aromatic potential, no differences clearly appeared.