IVAS 2022 banner
IVES 9 IVES Conference Series 9 IVAS 9 IVAS 2022 9 Carbon isotope ratio (Δ13C) and phenolic profile used to discriminate wines from Dealu mare and Cotnari regions (Romania)

Carbon isotope ratio (Δ13C) and phenolic profile used to discriminate wines from Dealu mare and Cotnari regions (Romania)

Abstract

Regarding the food quality, authenticity is one of the most important issues in the context of ensuring the safety and security of consumers, but is also more important when it comes to wine (one of the most counterfeited foods in the world).

A batch of 28 wines of Romanian varieties obtained in two regions well known for the production of wines from Romania (Dealu Mare and Cotnari) was analyzed from a physical-chemical point of view in order to discriminate them according to geographical origin and variety. The assessment of the carbon isotope ratio in ethanol extracted from wine provides relevant information to validate the geographical origin of wines. At the same time, the phenolic compounds in wine composition are of great importance, they contribute to the formation of characteristics such as taste, color and structure. The profile of these compounds is very different depending on grape variety, climatic conditions in each area and the applied wine-making technology. Therefore, a correlation between the carbon isotope ratio and the phenolic compounds profile can provide an overview of wines of a certain variety or region. Thus, the carbon isotope ratio (δ13C) was determined for all wines in this batch, which varied between -27.13 and -25.83 for wines from the Dealu Mare region and between -28.27 and -25.66 for wines from the Cotnari region. Also 12 phenolic compounds (gallic acid, protocathecic acid, caftaric acid, caffeic acid, coumaric acid, trans resveratrol, hydroxytyrosol, tyrosol, procyanidin dimer B1 and procyanidin dimer B2, catechin and epicatechin) were identified and quantified.
The δ13C measurements have been performed using an elemental analyser VarioMicroCube, Elementar coupled to an isotope ratio monitoring by mass spectrometry (Isoprime, Elementar) while the phenolic compounds content was analyzed by high-performance liquid chromatography (HPLC-PDA). In order to differentiate the wine samples according to the geographical region and the variety, statistical analysis was applied and thus a good discrimination of the wines according to the region and at the same time of the varieties within the same region was achieved.

DOI:

Publication date: June 23, 2022

Issue: IVAS 2022

Type: Article

Authors

Cotea Valeriu1, Popirda Andreea1, Luchian Camelia Elena1, Colibaba Lucia Cintia1, Focea Elena Cornelia1, Nicola Sebastien2 and Noret Laurence2

1Iasi University of Life Sciences, Faculty of Horticulture, Department of Horticultural Technologies, 3rd M. Sadoveanu Alley, 700490 Iasi, Romania
2Université Bourgogne Franche-Comté, AgroSup Dijon, PAM UMR A 02.102, Institut Universitaire de la Vigne et du Vin – Jules Guyot, F-21000 Dijon, France

Contact the author

Keywords

wine, geographical origin, δ13C measurements, phenolic compounds analysis

Tags

IVAS 2022 | IVES Conference Series

Citation

Related articles…

Impact of oenological tannins on microvinifications affected by downy mildew

AIM: Vine diseases are still responsible for economic losses. Previous study in our laboratory, have shown effects of oenological tannins against Botrytis cinerea1,2. According to this, the aim was to evaluate the wine protection by oenological tannins against an another disease, the downy mildew. METHODS: During the 2020 vintage, infected grapes by downy mildew (Vitis vinifera cv. Merlot) were collected from the dispositive ResIntBio. The 100 kg were crushed, destemmed and dispatch into 10 aluminium tanks. SO2 was added at 3 g/hL. Oenological tannins (grape, quebracho, ellagitannin or gallotannin) were added at 100 g/hL into eight different tanks (4×2 tanks). The two last tanks were considered as control without addition of oenological tannins. Alcoholic fermentation was achieved with Actiflore 33® at 20 g/hL. Malolactic fermentation was achieved with Lactoenos B7at 1 g/hL. Finished wines were sulfited to obtain 45 mg/L of total SO2.

Green Vineyards: skills development for wine industry personnel: responding to the challenges of climate change

A fair and sustainable society, with a modern, resource-efficient and competitive economy cannot be achieved without a workforce to support it.

Protected Designation of Origin (D.P.O.) Valdepeñas: classification and map of soils

The objective of the work described here is the elaboration of a map of the different types of vineyard soils that to guide the famers in the choice of the most productive vine rootstocks and varieties. 90 vineyard soils profiles were analysed in the entire territory of the Origen Denominations of Valdepeñas. The sampling was carried out in 2018 (June to October) by making a sampling grid, followed by photointerpretation and control in the field. The studied soils can be grouped into 9 different soil types (according to FAO 2006 classification): Leptosols, Regosols, Fluvisols, Gleysols, Cambisols, Calcisols, Luvisols and Anthrosols. A map showing the soil distribution with different type of soils has been made with the ArcGIS program. Regarding to the choice of rootstock, Calcisoles are soils with a high active limestone content, so the rootstocks used in these soils must be resistant to this parameter; Luvisols are deep soils with high clay content, so they will support vigorous rootstocks. Because the cartographic units are composed of two or more subgroups, with are associated in variable proportions, 9 different soil associations have been established; Unit 1: Leptosols, Cambisols and Luvisols (80%, 15% and 5% respectively); Unit 2: Cambisols with Regosols and Luvisols (40%, 30% and 30% respectively); Unit 3: Cambisols and Gleysols with Regosols (40%, 40% and 20% respectively); Unit 4: Regosols with Cambisols, Leptosols and Calcisols (40%, 30%, 15% and 15% respectively); Unit 5: Cambisols, Leptosols, Calcisols and Regosols (25% each of them); Unit 6: Luvisols with Cambisol and Calcisols (80%, 10% and 10% respectively); Unit 7: Luvisols and Calcisols with Cambisols (40%, 40% and 20% respectively); Unit 8: Calcisols with, Cambisols and Luvisols (80%, 10% and 10% respectively); Unit 9: Anthrosols. These study allow to elaborate the first map of vineyard soils of this Protected Designation of Origin in Castilla-La Mancha.

Grouping Vitis vinifera grapevine varieties based on their aromatic composition

Climate change is likely to impact wine typicity across the globe, raising concerns in wine regions historically renowned for the quality of their terroir1. Amongst several changes in viticultural practices, replacing some of the planting material (i.e. clones, rootstocks and cultivars) is thought to be one of the most promising potential levers to be used for adapting to climate change. But the change of cultivars also involves the issue of protecting the region’s wine typicity. In Bordeaux (France), extensive research has been conducted on identifying meridional varieties that could be good candidates to help guard against the effects of climate change2 while less research has been done concerning their impacts on Bordeaux wine typicity.

Ten grapevine rootstocks: effects on vegetative development, production and grape quality of cv. Mencia in the d.o. Bierzo (Spain)

Grapevine rootstock is basic to achieve good adaptation of the vine to ground and environment.