WAC 2022 banner
IVES 9 IVES Conference Series 9 WAC 9 WAC 2022 9 3 - WAC - Posters 9 Effects of oak barrel aging monitored by 1H-NMR metabolomics

Effects of oak barrel aging monitored by 1H-NMR metabolomics

Abstract

The study of wine evolution during barrel aging is an important aspect of wine quality. Our previous works have shown that wine metabolome monitoring by

1H-NMR approaches allows determining the impact of different winemaking processes including traitements using enzymes or finning agents [1]. In this study, the effects of oak barrel aging were investigated by 1H-NMR metabolomics. Targeted and untargeted 1H-NMR analyses were performed on wines conserved in barrels provided by four different barrel manufacturers. Wine samples were taken after one and twelve months. The collected data were statistically processed by principal component analysis (PCA), partial least squares discriminant analysis (PLS-DA), and partial orthogonal least squares discriminant analysis (OPLS-DA). Cross permutation tests and ANOVA were performed to validate the results and determine the compounds significantly impacted. The results of chemometrics analyses show the relevance of 1H-NMR metabolomics for studying the impact of oak barrel aging. The targeted analysis allowed us to identify the compounds that evolved during barrel aging. The untargeted analysis proved to be particularly interesting for the study of the specific signature of each barrel makers. 1H-NMR metabolomics is a rapid method that could be used as a decision support tool for winemaking.

DOI:

Publication date: June 27, 2022

Issue: WAC 2022

Type: Article

Authors

Tristan Richard, Gregory Da Costa, Inès Le Mao

Presenting author

Tristan Richard – Université de Bordeaux, Œnologie EA 4577, USC 1366 INRA, INP, ISVV, 210 chemin de Leysotte, 33882 Villenave d’Ornon, France

Contact the author

Keywords

Barrel aging, NMR, metabolomics, chemiometrics

Tags

IVES Conference Series | WAC 2022

Citation

Related articles…

Influence of the “terroir” (soil, climate and wine grower) on the quality of red Grenache wines in the Rhône Valley

«L’Observatoire Grenache» est un réseau de parcelles qui a été mis en place par l’Institut Rhodanien en Vallée du Rhône sur les millésimes de 1995 à 1999. Composé de 24 parcelles de Vitis vinifera L. cv Grenache noir, ce réseau vise à étudier l’influence du terroir (sol, climat et vigneron) sur la qualité des vins. Les parcelles ont été choisies afin de représenter différentes situations géographiques et géopédologiques de la vallée du Rhône. Le matériel végétal (clone, porte-greffe), la taille (cordon de Royat), la densité et l’âge de la parcelle ont été encadrées. Ainsi les conditions de milieu (sol, climat) et les pratiques du vigneron étaient les principales sources de variations.

Enhancing hydric stress tolerance by editing the VviMYB60 promoter with CRISPR/Cas9 

Climate change presents increasing challenges to viticulture, particularly with rising water stress contributing significantly to yield losses and damages. The identification of the MYB60 transcription factor, which regulates stomatal opening and closing in Arabidopsis thaliana and Vitis vinifera, offers potential solutions. Notably, knockout studies in Arabidopsis have shown reduced stomatal opening and increased drought tolerance in myb60 mutants. Additionally, the grapevine ortholog, VviMYB60, can restore the wild-type phenotype of Arabidopsis myb60 mutants. Further investigation of the Arabidopsis promoter region has revealed that mutations in DOF motifs lead to reduced expression of AtMYB60.

Streamlining rootstock selection: new indices for efficiency and stability in viticulture

Grapevine rootstocks play a pivotal role in influencing scion vigor, yield, and fruit quality, making their selection critical for sustainable vineyard management.

AGEING BOTTLED WINES SUBMERGED IN SEA: DOES IT IMPACT WINE COMPOSITION?

Aging wines is a common practice in oenology, which in recent years has undergone some innovations. Currently, we are witnessing the practice of aging bottled wine in depth, immersed in the sea or in reservoirs, for variable periods of time, but so far, little is known about the impact of aging in depth on the physicochemical properties, of wines.
The objective of this work was to evaluate the impact of this practice on the physicochemical characteristics, in particular to verify changes in the volatile composition of wines bottled and subsequently immersed in depth. A red wine from Cabernet Sauvignon was bottled and a set of bottles were submerged from July to February (2020), another set of bottles were submerged from February to September (2020) and another set was kept in the wine cellar. Bottles from each set were analyzed (in triplicate) in July 2021.

White grape must processed by UHPH as an alternative to SO2 addition: Effect on the phenolic composition in three varieties

The quantity and distribution of polyphenols in musts play a fundamental role in the white winemaking. This is because these substances are exposed to oxidation reactions, which are catalysed by the polyphenol oxidase (PPO), leading to a decrease in the quality of the wines produced. PPO is inactivated by SO2, but currently, due to the restrictions of the legislation, other methodologies are being investigated. Ultra-High Pressure Homogenization (UHPH) is a non-thermal physic technology that exerts an ultrahigh pressure pumping (>200 MPa) of a fluid through a valve in a continuous system.