WAC 2022 banner
IVES 9 IVES Conference Series 9 WAC 9 WAC 2022 9 3 - WAC - Posters 9 Effects of oak barrel aging monitored by 1H-NMR metabolomics

Effects of oak barrel aging monitored by 1H-NMR metabolomics

Abstract

The study of wine evolution during barrel aging is an important aspect of wine quality. Our previous works have shown that wine metabolome monitoring by

1H-NMR approaches allows determining the impact of different winemaking processes including traitements using enzymes or finning agents [1]. In this study, the effects of oak barrel aging were investigated by 1H-NMR metabolomics. Targeted and untargeted 1H-NMR analyses were performed on wines conserved in barrels provided by four different barrel manufacturers. Wine samples were taken after one and twelve months. The collected data were statistically processed by principal component analysis (PCA), partial least squares discriminant analysis (PLS-DA), and partial orthogonal least squares discriminant analysis (OPLS-DA). Cross permutation tests and ANOVA were performed to validate the results and determine the compounds significantly impacted. The results of chemometrics analyses show the relevance of 1H-NMR metabolomics for studying the impact of oak barrel aging. The targeted analysis allowed us to identify the compounds that evolved during barrel aging. The untargeted analysis proved to be particularly interesting for the study of the specific signature of each barrel makers. 1H-NMR metabolomics is a rapid method that could be used as a decision support tool for winemaking.

DOI:

Publication date: June 27, 2022

Issue: WAC 2022

Type: Article

Authors

Tristan Richard, Gregory Da Costa, Inès Le Mao

Presenting author

Tristan Richard – Université de Bordeaux, Œnologie EA 4577, USC 1366 INRA, INP, ISVV, 210 chemin de Leysotte, 33882 Villenave d’Ornon, France

Contact the author

Keywords

Barrel aging, NMR, metabolomics, chemiometrics

Tags

IVES Conference Series | WAC 2022

Citation

Related articles…

Monitoring of microbial biomass to characterise vineyard soils

Le sol est un facteur important permettant la croissance de la vigne. Les propriétés physiques et chimiques, mais aussi microbiologiques ont une influence sur beaucoup des fonctions du sol comme la structure, le drainage, la fertilité, déterminant la vigueur des plantes et le potentiel œnologique des raisins.

Contribution of soil for tipifiyng wines in four geographical indications at Serra Gaúcha, Brazil

Brazil has a recent history on geographical indications and product regulation for high quality wines. The first geographic indication implemented was the Vale dos Vinhedos Indication of Procedence (

Techniques of delimitation in France

La pratique de la délimitation des aires des Appellations d’Origine Contrôlées françaises découle de la définition de la notion de terroir en Appellation

Combined abiotic-biotic plant stresses on the roots of grapevine

In the 19th century, devastating outbreaks of phylloxera (Daktulosphaira vitifoliae Fitch), almost brought European viticulture to its knees. Phylloxera does not only take energy in form of sugars from the vine, but also affects the up- and down- regulations of genes, acts as a carbon sink and reprograms the physiology of the grapevines, including nutrient uptake and the defense system [1]. A key trait of rootstocks is the ability to perform well under high lime conditions as about 30 % of the land surface has calcareous soil. Iron deficiency not only causes the well-known problems of lime-induced chlorosis and stunted growth, but also affects the entire plant metabolism.

Sustainable fertilisation of the vineyard in Galicia (Spain)

Excessive fertilization of the vineyard leads to low quality grapes, increased costs and a negative impact on the environment. In order to establish an integrated management system aimed at a sustainable fertilization of the vineyards, nutritional reference levels were established. For this purpose, 30 representative vineyards of the Albariño variety were studied, in which soil and petiole analyses were carried out for two years and grape yield and quality at harvest were measured. In both years of study, soil pH, calcium, sodium and cation exchange capacity were positively correlated with calcium content and negatively correlated with manganese in grapes. Irrigated vineyards had higher levels of aluminium in soil and lower levels of calcium in petiole. Climatic conditions were very different in the years of the study. The year 2019 was colder than usual, in 2020 there was a marked water stress with high summer temperatures. This resulted in medium-high acidity in grapes in 2019 and low acidity in 2020, with sugar levels being similar both years. A very marked decrease in must amino nitrogen was observed in 2020, with ammonia nitrogen remaining stable. The correlation of acidity and sugar values in grapes with soil and petiole analysis data made it possible to establish reference levels for the nutritional diagnosis of the Albariño variety in this region. Based on these results, an easy-to-use TIC application is currently being created for grapegrowers, aimed at improving the sustainability of the vineyard through reasoned fertilization. This study has now been extended to other Galician vine varieties.