OENO IVAS 2019 banner
IVES 9 IVES Conference Series 9 OENO IVAS 9 OENO IVAS 2019 9 Analysis and composition of grapes, wines, wine spirits 9 Changes in red wine composition during bottle aging: impacts of viticultural conditions and oxygen availability

Changes in red wine composition during bottle aging: impacts of viticultural conditions and oxygen availability

Abstract

Bottle ageing is considered essential for most premium red wine production. An important aim of bottle ageing of wine is to achieve a balance between the oxidative and reductive development. This is typically evaluated by the accumulation of aldehyde compounds (causing oxidative off-flavour) and sulfur-containing compounds (causing reductive off-flavour) in the wine [1]. Although studies have been performed using variable amounts of oxygen available to the wine during bottle ageing, the impacts of viticultural practices on ageing processes have been studied less. 

This research investigated the impacts of viticultural conditions (2 grape varieties, 2 vineyard locations and 2 fruit maturities) and variable bottle ageing conditions (3 oxygen availability regimes and 4 bottle ages) on red wine composition, with a particular focus on the production of aldehyde and sulfur-containing compounds in wine. Analysis of the total concentrations of the key aroma compounds was performed by LC-QQQ-MS (aldehyde compounds in their hydroxyalkylsulfonate forms), HS-GC-SCD (sulfur-containing compounds) and HS-SPME-GC-MS (esters, C6 compounds and terpenes). After 24-month of ageing, all of the measured sulfur-containing compounds showed increased concentrations in all wines. 

For the wines made from the same grape (i.e. same variety, vineyard and harvest date), the high oxygen availability treatments contained lower concentrations of sulfur-containing compounds compared to the low oxygen treatments. Generally, methional, 2-methylpropanal, 3-methylbutanal, 5-methylfurfural and furfural exhibited increased concentrations with time, while phenylacetaldehyde, benzaldehyde and hexanal showed decreased concentrations. 

Chemometrics analysis showed that based on the compositional analysis, samples could be separated primarily based on wine ageing and the viticultural conditions adopted. Regardless of the oxygen regimes or the ageing time during the bottle ageing, the samples could be always separated according to the viticultural conditions of the grape. These results indicate the importance of the viticultural conditions of the grape on the ageing of wine, despite the extent of ageing or oxygen exposure. 

[1] Ugliano, M. Oxygen contribution to wine aroma evolution during bottle aging. 2013. Journal of Agricultural and Food Chemistry. 61(26): 6125-6136. 

DOI:

Publication date: June 11, 2020

Issue: OENO IVAS 2019

Type: Article

Authors

Xinyi Zhang, Nikolaos Kontoudakis, Katja Šuklje, Guillaume Antalick, John Blackman, Andrew Clark

Charles Sturt University, National Wine and Grape Industry Centre Locked Bag 588 – Boorooma St. Wagga Wagga NSW 2678 – Australia

Contact the author

Keywords

bottle ageing, viticultural conditions, oxidative-reductive development 

Tags

IVES Conference Series | OENO IVAS 2019

Citation

Related articles…

Ageing of sweet wines: oxygen evolution according to bung and barrel type

Barrel ageing is a crucial step in the wine process because it allows many changes to the wine as enrichment, colour stabilization, clarification and also a slow oxygenation. Effects of the oak barrel have to be known to prevent oxidation of the wine. The type of bung used during ageing is also a parameter to consider. Ageing sweet wines in barrel is a real challenge. These wines may need some oxygen at the beginning of ageing but they should be protected at the end of their maturation, to avoid oxidation.

SO2 consumption in white wine oxidation: approaches to low-input vinifications based on rapid electrochemical analyses and predictive enology

Oxidative stability is a critical factor in wine shelf-life. SO₂ is commonly added to wine due to its strong antioxidant activity, although there is a general push to reduce SO₂ use in vinification.

Mechanization of pre-flowering leaf removal under the temperate-climate conditions of Switzerland

Grapevine leaf removal (LR) in the cluster area is typically done between fruit set and cluster closure to create an unfavorable microclimate for fungal diseases, such as Botrytis cinerea and powdery mildew. Grape growers are now turning their attention to pre-flowering LR, which has additional benefits under certain conditions. When applied before flowering, LR strongly affects fruit set and thus the number of berries per cluster. It is therefore a good yield control tool, replacing time-consuming manual cluster thinning (Poni et al. 2006). It also improves berry structure, that is, skin thickness, skin-to-pulp ratio, and berry composition (total soluble solids, titratable acidity, and polyphenols) (Palliotti et al. 2012; Komm and Moyer 2015). By exacerbating competition for assimilates between reproductive and vegetative organs, pre-flowering LR also poses some risks. Excessive yield loss at the same year’s harvest due to a too low fruit set rate is the main concern: intensive pre-flowering LR (100% of the cluster area) can induce up to 50% yield loss in potted vines (Poni et al. 2005). Other parameters, such as cool climatic conditions during flowering, also affect fruit set rate and make it difficult to predict potential yield at harvest. Repeated and overly intensive preflowering LR can have repercussions over time and induce a decline in bud fruiting and plant vigor (Risco et al. 2014).

Evaluation of intra-vineyard spatial and temporal variability of leaf area index using multispectral images obtained by satellite (Landsat 8, Sentinel-2) and unmanned aerial vehicle platforms

Estimation of vineyard leaf area index (LAI) is an important aspect for the winegrowers. However, tracking and monitoring are difficult tasks due to time constraints. Satellite and unmanned aerial vehicle (UAV) imaging have become a practical monitoring method for LAI. Nevertheless, for a proper LAI determination, the image’s spatial resolution is a key factor, since low-resolution images are incapable of distinguishing between adjacent vines due to the large area covered in each pixel, this leads to misinterpretation or generalisation of vineyard information.

Attractiveness and sweetness of red wines: Synergies between American oak barrels and mannoproteins

In partnership with a Bordeaux property wanting to improve the quality of its second wine, the effects of two factors, American oak barrels and mannoproteins were studied. Their impact on the attractiveness and sweetness of wines were characterized during two successive vintages (2012 and 2013). Vinification took place with a homogeneous batch of Cabernet Sauvignon. The wine was then divided up into various groups of five barrels of French and American oak, new or reused. Analyses of volatile and non-volatile wood compounds were undertaken at four months and eight months of wood ageing, by LC-MS and GC-MS.