terclim by ICS banner
IVES 9 IVES Conference Series 9 UNCOVERING THE ROLE OF BERRY MATURITY STAGE AND GRAPE GENOTYPE ON WINE CHARACTERISTICS: INSIGHTS FROM CHEMICAL CHARACTERISTICS AND VOLATILE COMPOUNDS ANALYSIS

UNCOVERING THE ROLE OF BERRY MATURITY STAGE AND GRAPE GENOTYPE ON WINE CHARACTERISTICS: INSIGHTS FROM CHEMICAL CHARACTERISTICS AND VOLATILE COMPOUNDS ANALYSIS

Abstract

In a climate change context and aiming for sustainable, high-quality Bordeaux wine production, this project examines the impact of grape maturity levels in various cultivars chosen for their adaptability, genetic diversity, and potential to enhance wine quality. The study explores the effects on wine composition and quality through sensory and molecular methods. We studied eight 14-year-old Vitis vinifera cv. grape varieties from the same area (VITADAPT plots 1 and 5): Cabernet Franc, Cabernet Sauvignon, Carmenère, Castets, Cot, Merlot, Petit Verdot, and Touriga Nacional. We examined three berry maturity stages from the 2022 vintage: mid-veraison (MV), mid-maturity (MM), 7 days before maturity (M-7), at maturity (M), and 10 days post-maturity (M+10). Classical composition parameters were monitored during maturation. Fine volatile compounds, including lactones, furanones, norisoprenoids, and carbonyls as ripening and over-ripening markers, were quantified in grapes and wines using SPME-GC-MS, while thiols were analyzed in wines by SPE-GC-MS/MS. For example, according to the maturity stages, a significant increase in alcohol content was observed, which varied depending on the grape genotype. The highest concentrations were found in Petit Verdot (13.78 g/L in M-7), Cabernet Sauvignon, Merlot, and Petit Verdot (15.21, 15.30, and 15.75 g/L in M) and Merlot (16.68 g/L in M+10). These values were directly related to the higher sugar concentrations found in their must during the evaluated periods. Total acidity and pH levels vary among cultivars and are also influenced by different maturation stages. Some cultivars show more significant changes over time, while others display more modest fluctuations. As expected, the pH values and total acidity in wines from different cultivars were inversely related. Concerning the analyzed volatile compounds, surprisingly, Petit Verdot exhibited the highest concentrations of γ-nonalactone, followed by Cabernet Sauvignon and Cot, at all maturity stages including M-7 (6.39, 3.90, 3.61 µg/L), M (20.98, 8.98, 6.05 µg/L), and M+10 (13.93, 12.40, 8.48 µg/L), respectively. Overall, this study offers a new method to assess varieties’ sensitivity to overripening and vital insights into the impact of berry maturity stage and cultivar on wine physicochemical traits and volatile compound profiles. These findings can be a foundation for future research aiming to predict or model wine’s chemical and sensory properties.

 

1. Wang, Lina, et al. “Regulation of anthocyanin and sugar accumulation in grape berry through carbon limitation and exoge-nous ABA application.” Food Research International 160 (2022): 111478.
2. Pons, Alexandre, et al. “Impact of the Closure Oxygen Transfer Rate on Volatile Compound Composition and Oxidation Aroma Intensity of Merlot and Cabernet Sauvignon Blend: A 10 Year Study.” Journal of Agricultural and Food Chemistry (2022).
3. Van Leeuwen, Cornelis, et al. “How terroir shapes aromatic typicity in grapes and wines (Part I): Sourced from the research article:” Recent advancements in understanding the terroir effect on aromas in grapes and wines”(OENO One, 2020). Original language of the article: English.” IVES Technical Reviews, vine and wine (2023).
4. Darriet, Philippe, et al. “Aroma and aroma precursors in grape berry.” The biochemistry of the grape berry (2012): 111-136.

DOI:

Publication date: February 9, 2024

Issue: OENO Macrowine 2023

Type: Poster

Authors

Jacqueline Santos¹, Sabine Guilhaume¹, Cécile Thibon², Alexandre Pons²

1. UMR EGFV, Bordeaux Sciences Agro, INRA, University of Bordeaux, ISVV, Villenave d’Ornon, France.
2. Unitéde recherche Oenologie, EA 4577, USC 1366 INRA, ISVV, Universitéde Bordeaux, Bordeaux INP, F33882 Villenave d’Ornon France

Contact the author*

Keywords

Volatiles compounds, SPME-GC-MS, Composition parameters, Grape maturity

Tags

IVES Conference Series | oeno macrowine 2023 | oeno-macrowine

Citation

Related articles…

‘TROPICAL’ POLYFUNCTIONAL THIOLS AND THEIR ROLE IN AUSTRALIAN RED WINES

Following anecdotal evidence of unwanted ‘tropical’ character in red wines resulting from vineyard interventions and a subsequent yeast trial observing higher ‘red fruit’ character correlated with higher thiol concentrations, the role of polyfunctional thiols in commercial Australian red wines was investigated.
First, trials into the known tropical thiol modulation technique of foliar applications of sulfur and urea were conducted in parallel on Chardonnay and Shiraz.1 The Chardonnay wines showed expected results with elevated concentrations of 3-sulfanylhexanol (3-SH) and 3-sulfanylhexyl acetate (3-SHA), whereas the Shiraz wines lacked 3-SHA. Furthermore, the Shiraz wines were described as ‘drain’ (known as ‘reductive’ aroma character) during sensory evaluation although they did not contain thiols traditionally associated with ‘reductive’ thiols (H2S, methanethiol etc.).

REDUCING NITROGEN FERTILIZATION ALTERS PHENOLIC PROFILES OF VITIS VINIFERA L. CV. CABERNET GERNISCHT WINE OF YANTAI, CHINA

Nitrogen (N) fertilizer is important for grape growth and the quality of wine. It is essential to address the mismatch between N application and wine composition. Cabernet Gernischt (Vitis vinifera L.), as one of the main wine-grape cultivars in China, was introduced to Yantai wine region in 1892. This grape cultivar is traditionally used for quality dry red wine with fruit, spices aroma, ruby red and full-bodied wines. In order to regulate vine growth and improve grape and wine quality, Cabernet Gernischt grapevines were subjected to decreased levels of N treatments, compared to normal N supply treatment, during grape growing seasons of 2019 and 2020.

Overhead spray water treatment as a mitigation strategy for reducing vine stress and preserving grape quality during heatwaves

Changes in climate have been influencing the quality of wine grapes worldwide. The impact of extreme climate events over short periods is increasingly recognized as a serious risk to grape quality and yield quantity. In this study the mitigation effects of a pulsed water spray on vine canopy during heatwave events has been evaluated for maintaining vine condition during the growing season and grape quality. Vines of three varieties (Malbec, Bonarda, and Syrah) under drip irrigation in the UNCuyo experimental vineyard were treated with an overhead pulsed water spray.

TOWARDS THE SHELF-LIFE PREDICTION OF OLD CHAMPAGNE VINTAGES DEPENDING ON THE BOTTLE CAPACITY

Today, nearly one billion bottles of different sizes and capacities are aging in Champagne cellars while waiting to be put on the market. Among them, several tens of thousands of prestigious cuvees elaborated prior the 2000s are potentially concerned by prolonged aging on lees. However, when it comes to champagne tasting, dissolved CO₂ is a key compound responsible for the very much sought-after effer-vescence in glasses [1]. Yet, the slow decrease of dissolved CO₂ during prolonged aging of the most prestigious cuvees raises the issue of how long a champagne can age before it becomes unable to form CO₂ bubbles during tasting [2].

ANTHOCYANINS EXTRACTION FROM GRAPE POMACE USING EUTECTIC SOLVENTS

Grape pomace is one of the main by-products generated after pressing in winemaking.Emerging methods, such as ultrasound-assisted extraction with eutectic mixtures, have great potential due to their low toxicity, and high biodegradability. Choline chloride (ChCl) was used as a hydrogen bond acceptor and its corresponding hydrogen bond donor (malic acid, citric acid, and glycerol: urea). Components were heated at 80 °C and stirred until a clear liquid was obtained. Distilled water was added (30 % v/v). A solid-liquid ratio of 1 g pomace per 10 ml of eutectic solvent was used.