terclim by ICS banner
IVES 9 IVES Conference Series 9 OPTIMISATION OF THE AROMATIC PROFILE OF UGNI BLANC WINE DISTILLATE THROUGH THE CONTROL OF ALCOHOLIC FERMENTATION

OPTIMISATION OF THE AROMATIC PROFILE OF UGNI BLANC WINE DISTILLATE THROUGH THE CONTROL OF ALCOHOLIC FERMENTATION

Abstract

The online monitoring of fermentative aromas provides a better understanding of the effect of temperature on the synthesis and the loss of these molecules. During fermentation, gas and liquid phase concentrations as well as losses and total productions of volatile compounds can be followed with an unprecedented acquisition frequency of about one measurement per hour. Access to instantaneous production rates and total production balances for the various volatile compounds makes it possible to distinguish the impact of temperature on yeast production (biological effect) from the loss of aromatic molecules due to a physical effect³. Up to now, this innovative approach has been carried out successfully on isothermal fermentations1,2. Elucidating the role of anisothermal fermentation temperature profiles is a crucial issue that may lead to a deeper understanding of the influence of temperature on yeast metabolism in relation to the synthesis of aromatic molecules. In this study, results from different temperature control strategies of fermentation with increasing and decreasing profiles are explored. These fermentations were carried out on a laboratory scale with the online monitoring tool for alcoholic fermentation leading to a powerful dataset concerning higher alcohols, acetate and ethyl esters. The anisothermal control of the fermentation temperature shows that the production of higher alcohols is slowed down with the lowering of the temperature profiles and inversely for the ascending profiles. For isoamyl acetate and ethyl hexanoate, with ascending temperature profiles, larger losses are entailed with increasing temperature during fermentation and therefore the concentration in the liquid decreases. Obviously, the phenomenon is reversed for the descending profiles which allow to combine a better production of esters with an optimized conservation in liquid phase until the end of the alcoholic fermentation while minimizing the synthesis of higher alcohols. In strong concentrations, these alcohols may represent an organoleptic defect, especially for the distillation wines in Charente⁴. After the fermentation step, the wines were microdistilled with their lees in order to reproduce the conditions of distillation in Charente. Thanks to this step, it was possible to note the aromatic richness of the lees concerning the heavy ethyl esters⁵. Moreover, the impact of the anisothermal temperature profiles quoted above is also confirmed on the aromas released from the lees by the heating process of the distillation.

 

1. Mouret, J. R.; Perez, M.; Angenieux, M.; Nicolle, P.; Farines, V.; Sablayrolles, J. M. Online-Based Kinetic Analysis of Higher Alcohol and Ester Synthesis During Winemaking Fermentations. Food Bioprocess Technol 2014, 7 (5), 1235–1245. https://doi. org/10.1007/s11947-013-1089-5.
2. Mouret, J. R.; Camarasa, C.; Angenieux, M.; Aguera, E.; Perez, M.; Farines, V.; Sablayrolles, J. M. Kinetic Analysis and Gas–Liquid Balances of the Production of Fermentative Aromas during Winemaking Fermentations: Effect of Assimilable Nitrogen and Temperature. Food Research International 2014, 62, 1–10. https://doi.org/10.1016/j.foodres.2014.02.044.
3. Mouret, J.-R.; Aguera, E.; Perez, M.; Farines, V.; Sablayrolles, J.-M. Study of Oenological Fermentation: Which Strategy and Which Tools? Fermentation 2021, 7 (3), 155. https://doi.org/10.3390/fermentation7030155.
4. Sarvarova, N. N.; Cherkashina, Yu. A.; Evgen’ev, M. I. Application of Chromatographic Methods to the Determination of Cognac Quality Indicators. Journal of Analytical Chemistry 2011, 66 (12), 1190–1195. https://doi.org/10.1134/S1061934811120094.
5. Saerens, S. M. G.; Delvaux, F.; Verstrepen, K. J.; Van Dijck, P.; Thevelein, J. M.; Delvaux, F. R. Parameters Affecting Ethyl Es-ter Production by Saccharomyces Cerevisiae during Fermentation. Applied and Environmental Microbiology 2008, 74 (2), 454–461. https://doi.org/10.1128/AEM.01616-07.

DOI:

Publication date: February 9, 2024

Issue: OENO Macrowine 2023

Type: Poster

Authors

Charlie Guittin1,2, Faïza Maçna¹, Christian Picou¹, Marc Perez¹, Adeline Barreau², Xavier Poitou², Jean-Roch Mouret¹, Vincent Farines¹

1. SPO, Univ Montpellier, INRAE, Institut Agro, Montpellier, France
2. R&D department, Jas Hennessy & Co, Cognac, France

Contact the author*

Keywords

Online monitoring of aromas, Anisothermal temperature, Lees, Distillation

Tags

IVES Conference Series | oeno macrowine 2023 | oeno-macrowine

Citation

Related articles…

EVIDENCE OF THE INTERACTION OF ULTRASOUND AND ASPERGILLOPEPSINS I ON UNSTABLE GRAPE PROTEINS

Most of the effects of ultrasound (US) result from the collapse of bubbles due to cavitation. The shockwave produced is associated with shear forces, along with high localised temperatures and pressures. However, the high-speed stream, radical species formation, and heat generated during sonication may also affect the stability of some enzymes and proteins, depending on their chemical structure. Recently, Ce-lotti et al. (2021) reported the effects of US on protein stability in wines. To investigate this further, the effect of temperature (40°C and 70°C; 60s), sonication (20 kHz and 100 % amplitude, for 20s and 60s, leading to the same temperatures as above, respectively), in combination with Aspergillopepsins I (AP-I) supplementation (100 μg/L), was studied on unstable protein concentration (TLPs and chitinases) using HPLC with an UV–Vis detector in a TLPs-supplemented model system and in an unstable white wine.

THE POTENTIAL USE OF SOLUBLE POLYSACCHARIDES TO PREVENT THE OXIDATION OF ROSÉ WINES

Lately, rosé wine is rapidly increasing its popularity worldwide. Short-time macerations with the red skin of the grapes cause the partial extraction of anthocyanins, which are responsible for the pinki-sh-salmon hue of rosé wines. However, the low quantity of tannins (antioxidants) and richness in phenolic acids, which can be easily oxidized into yellowish pigments, tend to predispose rosé wines to an undesirable browning. Although the use of SO₂ for the prevention of oxidation is highly extended, this practice is expected to be reduced. Therefore, the search for alternative oenological adjuvants that prevent the oxidation and browning of rosé wines is highly desired.

DETERMINATION OF FREE AMINO ACIDS, AMINO ACID POTENTIAL AND PROTEASE ACTIVITY IN THE LEES AND STILL WINES OF CHAMPAGNE

Prior to winemaking, organic or mineral nitrogen compound concentrations are usually measured in the vineyard and in grape musts. These indicators facilitate vine cultivation decisions, usually through yield or vigor. During vinification, yeast and bacteria metabolize nitrogen compounds in the musts in order to generate biomass. After fermentation, the microorganisms rerelease a part of this nitrogen as soluble compounds into the wines. Another part remains bound in the lees and can be lost during racking. The must’s natural nitrogen quantities, additional supplements during fermentation, and lees contact management enhance the release of nitrogen compounds to the wines. During ageing these nitrogen compounds – primarily the amino acids – are implicated in the generation of odorous compounds such as heterocycles(1).

Overhead spray water treatment as a mitigation strategy for reducing vine stress and preserving grape quality during heatwaves

Changes in climate have been influencing the quality of wine grapes worldwide. The impact of extreme climate events over short periods is increasingly recognized as a serious risk to grape quality and yield quantity. In this study the mitigation effects of a pulsed water spray on vine canopy during heatwave events has been evaluated for maintaining vine condition during the growing season and grape quality. Vines of three varieties (Malbec, Bonarda, and Syrah) under drip irrigation in the UNCuyo experimental vineyard were treated with an overhead pulsed water spray.

MODULATION OF YEAST-DERIVED AROMA COMPOUNDS IN CHARDONNAY WINES USING ENCAPSULATED DIAMMONIUM PHOSPHATE TO CONTROL NUTRIENT RELEASE

Yeast-derived aroma compounds are the result of different and complex biochemical pathways that mainly occur during alcoholic fermentation. Many of them are related -but not limited- to the availability of nutrients in the fermentation medium and linked to nitrogen metabolism and biomass produced. Besides, the metabolic phase of yeast also regulates the expression of many enzymes involved in the formation of aroma active compounds. The work investigates the overall effect of continuous supplementation of nutrients during alcoholic fermentation of a grape must on the volatile composition of wines.