terclim by ICS banner
IVES 9 IVES Conference Series 9 OPTIMISATION OF THE AROMATIC PROFILE OF UGNI BLANC WINE DISTILLATE THROUGH THE CONTROL OF ALCOHOLIC FERMENTATION

OPTIMISATION OF THE AROMATIC PROFILE OF UGNI BLANC WINE DISTILLATE THROUGH THE CONTROL OF ALCOHOLIC FERMENTATION

Abstract

The online monitoring of fermentative aromas provides a better understanding of the effect of temperature on the synthesis and the loss of these molecules. During fermentation, gas and liquid phase concentrations as well as losses and total productions of volatile compounds can be followed with an unprecedented acquisition frequency of about one measurement per hour. Access to instantaneous production rates and total production balances for the various volatile compounds makes it possible to distinguish the impact of temperature on yeast production (biological effect) from the loss of aromatic molecules due to a physical effect³. Up to now, this innovative approach has been carried out successfully on isothermal fermentations1,2. Elucidating the role of anisothermal fermentation temperature profiles is a crucial issue that may lead to a deeper understanding of the influence of temperature on yeast metabolism in relation to the synthesis of aromatic molecules. In this study, results from different temperature control strategies of fermentation with increasing and decreasing profiles are explored. These fermentations were carried out on a laboratory scale with the online monitoring tool for alcoholic fermentation leading to a powerful dataset concerning higher alcohols, acetate and ethyl esters. The anisothermal control of the fermentation temperature shows that the production of higher alcohols is slowed down with the lowering of the temperature profiles and inversely for the ascending profiles. For isoamyl acetate and ethyl hexanoate, with ascending temperature profiles, larger losses are entailed with increasing temperature during fermentation and therefore the concentration in the liquid decreases. Obviously, the phenomenon is reversed for the descending profiles which allow to combine a better production of esters with an optimized conservation in liquid phase until the end of the alcoholic fermentation while minimizing the synthesis of higher alcohols. In strong concentrations, these alcohols may represent an organoleptic defect, especially for the distillation wines in Charente⁴. After the fermentation step, the wines were microdistilled with their lees in order to reproduce the conditions of distillation in Charente. Thanks to this step, it was possible to note the aromatic richness of the lees concerning the heavy ethyl esters⁵. Moreover, the impact of the anisothermal temperature profiles quoted above is also confirmed on the aromas released from the lees by the heating process of the distillation.

 

1. Mouret, J. R.; Perez, M.; Angenieux, M.; Nicolle, P.; Farines, V.; Sablayrolles, J. M. Online-Based Kinetic Analysis of Higher Alcohol and Ester Synthesis During Winemaking Fermentations. Food Bioprocess Technol 2014, 7 (5), 1235–1245. https://doi. org/10.1007/s11947-013-1089-5.
2. Mouret, J. R.; Camarasa, C.; Angenieux, M.; Aguera, E.; Perez, M.; Farines, V.; Sablayrolles, J. M. Kinetic Analysis and Gas–Liquid Balances of the Production of Fermentative Aromas during Winemaking Fermentations: Effect of Assimilable Nitrogen and Temperature. Food Research International 2014, 62, 1–10. https://doi.org/10.1016/j.foodres.2014.02.044.
3. Mouret, J.-R.; Aguera, E.; Perez, M.; Farines, V.; Sablayrolles, J.-M. Study of Oenological Fermentation: Which Strategy and Which Tools? Fermentation 2021, 7 (3), 155. https://doi.org/10.3390/fermentation7030155.
4. Sarvarova, N. N.; Cherkashina, Yu. A.; Evgen’ev, M. I. Application of Chromatographic Methods to the Determination of Cognac Quality Indicators. Journal of Analytical Chemistry 2011, 66 (12), 1190–1195. https://doi.org/10.1134/S1061934811120094.
5. Saerens, S. M. G.; Delvaux, F.; Verstrepen, K. J.; Van Dijck, P.; Thevelein, J. M.; Delvaux, F. R. Parameters Affecting Ethyl Es-ter Production by Saccharomyces Cerevisiae during Fermentation. Applied and Environmental Microbiology 2008, 74 (2), 454–461. https://doi.org/10.1128/AEM.01616-07.

DOI:

Publication date: February 9, 2024

Issue: OENO Macrowine 2023

Type: Poster

Authors

Charlie Guittin1,2, Faïza Maçna¹, Christian Picou¹, Marc Perez¹, Adeline Barreau², Xavier Poitou², Jean-Roch Mouret¹, Vincent Farines¹

1. SPO, Univ Montpellier, INRAE, Institut Agro, Montpellier, France
2. R&D department, Jas Hennessy & Co, Cognac, France

Contact the author*

Keywords

Online monitoring of aromas, Anisothermal temperature, Lees, Distillation

Tags

IVES Conference Series | oeno macrowine 2023 | oeno-macrowine

Citation

Related articles…

CHANGES IN CU FRACTIONS AND RIBOFLAVIN IN WHITE WINES DURING SHORT-TERM LIGHT EXPOSURE: IMPACTS OF OXYGEN AND BOTTLE COLOUR

Copper in white wine can be associated with Cu(II) organic acids (Cu fraction I), Cu(I) thiol species (Cu fraction II), and Cu sulfides (Cu fraction III). The first two fractions are associated with the repression of reductive aromas in white wine, but these fractions gradually decrease in concentration during the normal bottle aging of wine. Although exposure of white wine to fluorescent light is known to induce the accumulation of volatile sulfur compounds, causing light-struck aroma, the influence on the loss of protective Cu fractions is uncertain. Riboflavin is known to be a critical initiator of photochemical reac-tions in wine, but the rate of its decay under short-term light exposure in different coloured bottles and for wine of different oxygen concentrations is not well understood.

EMERGENCE OF INORGANIC PHOSPHONATE RESIDUES IN GRAPEVINE PLANT PARTS, BERRIES AND WINES FROM SOURCES OTHER THAN FOLIAR SPRAYING

Inorganic phosphonates are known to effectively support the control of grapevine downy mildew in vi- ticulture. Their application helps the plant to induce an earlier and more effective pathogen defense. However, inorganic phosphonates have been banned in organic viticulture due to their classification as plant protection products since October 2013. Despite the ban, phosphonate has been recently detected in organic wines.

REVEALING THE ORIGIN OF BORDEAUX WINES WITH RAW 1D-CHROMATOGRAMS

Understanding the composition of wine and how it is influenced by climate or wine-making practices is a challenging issue. Two approaches are typically used to explore this issue. The first approach uses chemical
fingerprints, which require advanced tools such as high-resolution mass spectrometry and multidimensional chromatography. The second approach is the targeted method, which relies on the widely available 1-D GC/MS, but involves integrating the areas under a few peaks which ends up using only a small fraction of the chromatogram.

PHENOTYPIC DIVERSITY AND BIO-PROTECTION CAPABILITY OF METSCHNIKOWIA SP. IN OENOLOGY

Nowadays, the trend is to reduce the use of chemical inputs in the food sector, including in oenology. One of the inputs widely used in the wine making process are sulfites, for its several properties: antimicrobial and antioxidiant. This use isn’t without consequences on consumer’s health and environment, it can lead for example to allergic reactions and pollution. To limit the addition of chemical inputs, microbial alternatives are used. It consists to inoculate in grape must, a micro-organism able to inhibit the growth of the negative indigenous flora during the phase before the fermentation and to guarantee the sensory qualities of wines.

EFFECTIVENESS OF APPLIED MATERIALS IN REDUCING THE ABSORPTION OF SMOKE MARKER COMPOUNDS IN A SIMULATED WILDFIRE SCENARIO

Smoke taint (ST) is a grape-wine off-flavour that may occur when grapes absorb volatile phenols (VPs) originating from wildfire smoke (1). ST is associated with the negative sensory attributes such as smoky and ashy notes. VPs are glycosylated in the plant and thus present in both free and bound forms (2; 3). Wildfire smoke has resulted in a decline in grape and wine quality and financial losses which has become a prominent issue for the global wine industry.