terclim by ICS banner
IVES 9 IVES Conference Series 9 OPTIMISATION OF THE AROMATIC PROFILE OF UGNI BLANC WINE DISTILLATE THROUGH THE CONTROL OF ALCOHOLIC FERMENTATION

OPTIMISATION OF THE AROMATIC PROFILE OF UGNI BLANC WINE DISTILLATE THROUGH THE CONTROL OF ALCOHOLIC FERMENTATION

Abstract

The online monitoring of fermentative aromas provides a better understanding of the effect of temperature on the synthesis and the loss of these molecules. During fermentation, gas and liquid phase concentrations as well as losses and total productions of volatile compounds can be followed with an unprecedented acquisition frequency of about one measurement per hour. Access to instantaneous production rates and total production balances for the various volatile compounds makes it possible to distinguish the impact of temperature on yeast production (biological effect) from the loss of aromatic molecules due to a physical effect³. Up to now, this innovative approach has been carried out successfully on isothermal fermentations1,2. Elucidating the role of anisothermal fermentation temperature profiles is a crucial issue that may lead to a deeper understanding of the influence of temperature on yeast metabolism in relation to the synthesis of aromatic molecules. In this study, results from different temperature control strategies of fermentation with increasing and decreasing profiles are explored. These fermentations were carried out on a laboratory scale with the online monitoring tool for alcoholic fermentation leading to a powerful dataset concerning higher alcohols, acetate and ethyl esters. The anisothermal control of the fermentation temperature shows that the production of higher alcohols is slowed down with the lowering of the temperature profiles and inversely for the ascending profiles. For isoamyl acetate and ethyl hexanoate, with ascending temperature profiles, larger losses are entailed with increasing temperature during fermentation and therefore the concentration in the liquid decreases. Obviously, the phenomenon is reversed for the descending profiles which allow to combine a better production of esters with an optimized conservation in liquid phase until the end of the alcoholic fermentation while minimizing the synthesis of higher alcohols. In strong concentrations, these alcohols may represent an organoleptic defect, especially for the distillation wines in Charente⁴. After the fermentation step, the wines were microdistilled with their lees in order to reproduce the conditions of distillation in Charente. Thanks to this step, it was possible to note the aromatic richness of the lees concerning the heavy ethyl esters⁵. Moreover, the impact of the anisothermal temperature profiles quoted above is also confirmed on the aromas released from the lees by the heating process of the distillation.

 

1. Mouret, J. R.; Perez, M.; Angenieux, M.; Nicolle, P.; Farines, V.; Sablayrolles, J. M. Online-Based Kinetic Analysis of Higher Alcohol and Ester Synthesis During Winemaking Fermentations. Food Bioprocess Technol 2014, 7 (5), 1235–1245. https://doi. org/10.1007/s11947-013-1089-5.
2. Mouret, J. R.; Camarasa, C.; Angenieux, M.; Aguera, E.; Perez, M.; Farines, V.; Sablayrolles, J. M. Kinetic Analysis and Gas–Liquid Balances of the Production of Fermentative Aromas during Winemaking Fermentations: Effect of Assimilable Nitrogen and Temperature. Food Research International 2014, 62, 1–10. https://doi.org/10.1016/j.foodres.2014.02.044.
3. Mouret, J.-R.; Aguera, E.; Perez, M.; Farines, V.; Sablayrolles, J.-M. Study of Oenological Fermentation: Which Strategy and Which Tools? Fermentation 2021, 7 (3), 155. https://doi.org/10.3390/fermentation7030155.
4. Sarvarova, N. N.; Cherkashina, Yu. A.; Evgen’ev, M. I. Application of Chromatographic Methods to the Determination of Cognac Quality Indicators. Journal of Analytical Chemistry 2011, 66 (12), 1190–1195. https://doi.org/10.1134/S1061934811120094.
5. Saerens, S. M. G.; Delvaux, F.; Verstrepen, K. J.; Van Dijck, P.; Thevelein, J. M.; Delvaux, F. R. Parameters Affecting Ethyl Es-ter Production by Saccharomyces Cerevisiae during Fermentation. Applied and Environmental Microbiology 2008, 74 (2), 454–461. https://doi.org/10.1128/AEM.01616-07.

DOI:

Publication date: February 9, 2024

Issue: OENO Macrowine 2023

Type: Poster

Authors

Charlie Guittin1,2, Faïza Maçna¹, Christian Picou¹, Marc Perez¹, Adeline Barreau², Xavier Poitou², Jean-Roch Mouret¹, Vincent Farines¹

1. SPO, Univ Montpellier, INRAE, Institut Agro, Montpellier, France
2. R&D department, Jas Hennessy & Co, Cognac, France

Contact the author*

Keywords

Online monitoring of aromas, Anisothermal temperature, Lees, Distillation

Tags

IVES Conference Series | oeno macrowine 2023 | oeno-macrowine

Citation

Related articles…

EFFECTS OF LEAF REMOVAL AT DIFFERENT BUNCHES PHENOLOGICAL STAGES ON FREE AND GLYCOCONJUGATE AROMAS OF SKINS AND PULPS OF TWO ITALIAN RED GRAPES

Canopy-management practices are applied in viticulture to improve berries composition and quality, having a great impact on primary and secondary grape metabolism. Among these techniques, cluster zone leaf removal (defoliation) is widely used to manage air circulation, temperature and light radiation of grape bunches and close environment. Since volatiles are quantitatively and qualitatively influenced by the degree of fruit ripeness, the level of solar exposure, and the thermal environment in which grapes ripen, leaf removal has been shown to affect volatile composition of grape berries [1].

VOLATILE AND GLYCOSYLATED MARKERS OF SMOKE IMPACT: EVOLUTION IN BOTTLED WINE

Smoke impact in wines is caused by a wide range of volatile phenols found in wildfire smoke. These compounds are absorbed and accumulate in berries, where they may also become glycosylated. Both volatile and glycosylated forms eventually end up in wine where they can cause off-flavors. The impact on wine aroma is mainly attributed to volatile phenols, while in-mouth hydrolysis of glycosylated forms may be responsible for long-lasting “ashy” aftertastes (1).

ENRICHMENT OF THE OENOLOGICAL MALDI-TOF/MS PROTEIN SPECTRA DATABASE FOR RELIABLE OENOLOGICAL YEAST AND BACTERIA IDENTIFICATION

The Matrix Assisted Laser Desorption/Ionization–Time-Of-Flight Mass Spectrometry (MALDI-TOF MS) technology is commonly used in food and medical sector to identify yeast or bacteria species isolated from a nutritive culture media. Since a decade, brewery and oenology industries have been attracted to this method which combines fast analysis times, reliability and low cost of analysis. Briefly, this method is based on the comparison of the MALDI-TOF/MS protein spectra of an isolated colony of yeast or bacteria with those contain in a manufacturer’s reference protein spectra database. Initiated in 2015, the creation of the first oenological mass spectra database has proved to be essential for increase quality of species identification.

OENOLOGICAL TANNINS FOR PREVENTING THE LIGHT-STRUCK TASTE IN WHITE AND ROSÉ WINES

The light exposure of wine can be detrimental as a relevant loss of aromas takes place [1] and light-induced reactions can occur. The latter involves riboflavin (RF), a photosensitive compound, that is fully reduced by acquiring two electrons. When the electron-donor is methionine, the light-struck taste (LST) can appear leading to cooked cabbage, onion and garlic odours-like [2]. The use of oenological tannins can limit the appearance of LST in both model wine [3] and white wine [4]. This research aimed to evaluate the impact of certain oenological tannins, selected in a previous study as the most effective against LST [5], in both white and rosé wines.

STATISTICAL COMPARISON OF GROWTH PARAMETERS OF NINE BIOPROTECTION STRAINS IMPLEMENTED ON ARTIFICIALLY CONTAMINATED SYNTHETIC MUST

In recent years, consumer demand for products without chemical additives increased, becoming a priority for the wine sector. SO₂ is widely used for its multiple properties including antiseptics, antioxidants and antioxidasics and the strategy of bioprotection in winemaking represents now an alternative to this chemical additive. In oenology, results have highlighted the interest of bioprotection to limit the development of microorganisms like Hanseniaspora uvarum and thus reduce the doses of sulphite. Indeed, this species is considered because of its acetic acid and methyl butyl acetate production, the latter can cover the varietal character of wines.