terclim by ICS banner
IVES 9 IVES Conference Series 9 International Congress on Grapevine and Wine Sciences 9 2ICGWS-2023 9 Polyphenol content of cork granulates at different steps of the manufacturing process of microagglomerated stoppers treated with supercritical CO2 used for wine bottling

Polyphenol content of cork granulates at different steps of the manufacturing process of microagglomerated stoppers treated with supercritical CO2 used for wine bottling

Abstract

The wine closure industry is mainly divided into three categories: screw caps, synthetic closures, and cork-based closures. Among this latter, microagglomerated cork stoppers treated with supercritical CO2 are now widely used, especially to avoid cork taint contaminations[1]. They are designed with cork granules obtained from cork offcuts of the punching process during the natural cork stoppers production. A previous study[2] showed that these stoppers released fewer polyphenols in 12 % (v/v) hydroalcoholic solution than natural cork stoppers. Thus, the present study aims to understand in which step of the manufacturing process of microagglomerated cork stoppers, phenolic compounds are eliminated and which polyphenols are likely to migrate into the wine during horizontal storage. Therefore, granulates from three different steps of the manufacturing process and supercritical CO2 water extracts were analyzed regarding their polyphenolic compounds. Polyphenol extraction was performed on granulates (1g) using 80 mL of acetone/water (70/30, v/v) acidified at 0.1% HCOOH in order to achieve a total extraction of polyphenols. Granulate extracts were then evaporated until dryness and recovered with 20 mL of 0.1% HCOOH acidified water. Polyphenols of the resulting samples and the supercritical CO2 water extracts were quantified by HPLC-MS after filtering. The granulates were also extracted with 12% (v/v) ethanol/water to carry out a sensory profile and thus to highlight possible olfactory and/or gustative differences between granulates at the different steps of the manufacturing process.

Acknowledgements: The authors would like to thank Diam Bouchage (Céret, France) for its financial support and for providing samples of granulates and also Christophe Loisel for his expertise in microagglomerated cork manufacturing.

References
1) Taylor, M. K., Young, T. M., Butzke, C. E., & Ebeler, S. E. (2000). Supercritical fluid extraction of 2, 4, 6-trichloroanisole from cork stoppers. Journal of agricultural and food chemistry, 48(6): 2208‑2211, DOI 10.1021/jf991045q
2) Gancel, A.-L., Jourdes, M., Pons, & Teissedre P.-L. (2023). Polyphenol migration from natural and microagglomerated cork stoppers to hydroalcoholic solutions and their sensory impact. Oeno-one (accepted on 3 June 2023).

DOI:

Publication date: October 13, 2023

Issue: ICGWS 2023

Type: Poster

Authors

Anne-Laure Gancel1, 2, Michaël Jourdes1, 2, Alexandre Pons1, 2, 3 and Pierre-Louis Teissedre1, 2*

1 Univ. Bordeaux, Bordeaux INP, INRAE, OENO, UMR 1366, ISVV, F-33140 Villenave d’Ornon, France
2 Bordeaux Sciences Agro, F-33170 Gradignan, France
Tonnellerie Seguin-Moreau, ZI Merpins, 16103, Cognac, France

Contact the author*

Keywords

wine bottling, microagglomerated cork stoppers, cork granulates, manufacturing process, supercritical CO2, phenolic compounds, sensory analysis

Tags

2ICGWS | ICGWS | ICGWS 2023 | IVES Conference Series

Citation

Related articles…

Quantifying water use diversity across grapevine rootstock-scion combinations

Vines require proper light levels, temperature, and water availability, and climate change is modifying these factors, hampering yield and quality. Despite the large diversity of rootstocks, varieties, and clones, we still lack knowledge of their combined effects and potential role in a warmer and dryer future. Therefore, we aim to characterize some of the existing diversity of rootstocks and genotypes and their interaction at the eco-physiological level, combining stomatal conductance (gs) and chlorophyll a fluorescence analysis.

Influence of irrigation frequency on berry phenolic composition of red grape varieties cultivated in four spanish wine-growing regions

The global warming phenomenon involves the frequency of extreme meteorological events accompanied by a change in rainfall distribution. Irrigation frequency (IF) affects the spatial and temporal soil water distribution but its effects on the phenolic composition of the grape have been scarcely studied. The aim of this work was to evaluate the effects of four deficit irrigation frequencies of 30 % ETo: one irrigation per day (T01), two irrigations per week (T03), one irrigation per week (T07) and one irrigation every two weeks (T15) on berry phenolic composition at harvest.

High-throughput screening of physical-mechanical berry skin traits facilitates targeted selection of breeding material with resistance to Botrytis bunch rot and grape sunburn

The ongoing climate change implies an increasing mean air temperature, which is signified by weather extremes or sudden changes between drought and local heavy rainfalls. These changing conditions are especially challenging for the established grapevine varieties growing under cool climate conditions due to an increased risk for fungal diseases like downy mildew (DM) and Botrytis bunch rot (BBR) as well as for grape sunburn. To meet that demand, the scope of most grapevine breeding programs is the selection of mildew fungus-resistant and climatic adapted grapevines with balanced, healthy yield and outstanding wine quality.

What to do to solve the riddle of vine rootstock induced drought tolerance

Climate change will increase the frequency of water deficit situation in some European regions, by the increase of the evapotranspiration and the reduction of rainfalls during the growing cycle. This requires finding ways of adaptation, including the use of plant material which is more tolerant to drought. In addition to the varieties used as scions that result in the typicality of wines, rootstocks constitute a relevant way of adaptation to more stressful environmental conditions.

Grape pomace, an active ingredient at the intestinal level: Updated evidence

Grape pomace (GP) is a winemaking by-product particularly rich in (poly)phenols and dietary fiber, which are the main active compounds responsible for its health-promoting effects. GP-derived products have been proposed to manage cardiovascular risk factors, including endothelial dysfunction, inflammation, hypertension, hyperglycemia, and obesity. Studies on the potential impact of GP on gut health are much more recent. However, it is suggested that, to some extent, this activity of GP as a cardiometabolic health-promoting ingredient would begin in the gastrointestinal tract as GP components (i.e., (poly)phenols and fiber) undergo extensive catabolism, mainly by the action of the intestinal microbiota, that gives rise to low-molecular-weight bioactive compounds that can be absorbed and utilized by the body.