terclim by ICS banner
IVES 9 IVES Conference Series 9 ESTIMATING THE INITIAL OXYGEN RELEASE (IOR) OF CORK CLOSURES

ESTIMATING THE INITIAL OXYGEN RELEASE (IOR) OF CORK CLOSURES

Abstract

Many factors influence aging of bottled wine, oxygen transfer through the closure is included. The maximum uptake of wine before oxidation begins varies from 60 mg.L-¹ to 180 mg.L-1 for white and red wines respectively [1].

The process of bottling may lead to considerable amounts of oxygen. The actual contribution of the transfer through the closure system becomes relevant at the bottle storage, but the amounts are small compared to prepacking operations [2] and to the total oxygen attained during filling.

When corks are inserted in bottlenecks, there is initial oxygen released (IOR) due to the compression exerted to accommodate them in the volume of the bottleneck. Then starts contribution of the transfer between the closure and the glass together through the cork.

The initial release of oxygen is significant compared to the transfer through the cork itself and has been reported around 60% to 70% of the total oxygen ingress in a bottle after the first month and around 90% to 97% after the second, either for corks tested under dry or under wine contact condition [3]. In a study designed for sparkling corks, inerting procedure allowed to reduce the initial oxygen release by around 1.5mg [4]. An identical procedure is used in the scope of oxygen transfer measurements as a preparation for the corks [5].

The current work aims at estimating the IOR of natural corks. Natural corks of a superior grade, 49 mm length and 24 mm diameter, ready for use were purged with nitrogen for 3 months to displace oxygen from cork cells. Then corks were inserted in bottles with controlled bottlenecks and oxygen ingress monitored using the non-invasive methodology [3] for two months. At 64 days, it was observed that corks submitted to the purging procedure released 1.4 mg of oxygen less. In a preliminary experiment purging for 1 month, the reduction of oxygen ingress was around 7% more which suggests that the additional months did not change much oxygen from the cork cells.

The ongoing project aims to consolidate the estimation of the IOR value and to be extended to micro agglomerated cork stoppers.

 

1. Singleton, Vernon L. 1987. “Oxygen with Phenols and Related Reactions in Musts, Wines, and Model Systems: Observations and Practical Implications.” Am J Enol Vitic. 69-77. doi:10.5344/ajev.1987.38.1.69.
2. Reeves, Malcolm J. 2009. “Packaging and the Shelf Life of Wine.” Em Food Packaging and Shelf Life A Practical Guide, de Gordon L. Robertson, 231- 257. CRC Press. doi:10.1201/9781420078459-c13.
3. Ana C. Lopes Cardoso, Chandisree Rajbux, Cristina L. M. Silva, Fátima Poças. 2022. “Modelling oxygen ingress through cork closures. Impact of test conditions.” Journal of Food Engineering 331. doi:10.1016/j.jfoodeng.2022.111105.
4. B. Villedey, S. Callas, A. Descôtes. 2021. Le Vigneron Champenois, 54-69.
5. EXCELL, Laboratoire FRANCE. 2018. “Study of Oxygen Permeability of Technical Corks.” Test Report. Contract No.: N°2017-05- 013 – N°2017-09-001., Merignac.

DOI:

Publication date: February 9, 2024

Issue: OENO Macrowine 2023

Type: Poster

Authors

C. Mariana Machado¹ and Ana Lopes Cardoso¹

1. Cork Supply Portugal, S.A., Rua Nova do Fial, 102, 4535-465 São Paio de Oleiros, Portugal

Contact the author*

Keywords

Oxygen, Corks, Bottle, Wine

Tags

IVES Conference Series | oeno macrowine 2023 | oeno-macrowine

Citation

Related articles…

CONTRIBUTION OF VOLATILE THIOLS TO THE AROMA OF RIESLING WINES FROM THREE REGIONS IN GERMANY AND FRANCE (RHEINGAU, MOSEL, AND ALSACE)

Riesling wines are appreciated for their diverse aromas, ranging from the fruity fresh characters in young vintages to the fragrant empyreumatic notes developed with aging. Wine tasters often refer to Riesling wines as prime examples showcasing terroir, with their typical aroma profiles reflecting the geographical provenance of the wine. However, the molecular basis of the distinctive aromas of these varietal wines from major Riesling producing regions in Europe have not been fully elucidated. In this study, new lights were shed on the chemical characterization and the sensory contribution of volatile thiols to Riesling wines from Rheingau, Mosel, and Alsace. First, Riesling wines (n = 46) from the three regions were collected and assessed for their aroma typicality by an expert panel.

INFLUENCE OF THE NITROGEN / LIPIDS RATIO OF MUSTS ON THE REVELATION OF AROMATIC COMPOUNDS IN SAUVIGNON BLANC WINE

Production of volatile compounds by yeast is known to be modulated by must nitrogen. Nevertheless, various parameter of must quality have an impact on yeast fermentation. In this study we propose to evaluate the impact of nitrogen / lipids balance on a Sauvignon Blanc grape juice (Val de Loire).
Must was prepared from the same grapes at pilot scale. Three modalities were carried out: direct pressing, direct pressing with a pre-fermentation cold stabulation and pellicular maceration before pressing.

DETERMINATION OF FREE AMINO ACIDS, AMINO ACID POTENTIAL AND PROTEASE ACTIVITY IN THE LEES AND STILL WINES OF CHAMPAGNE

Prior to winemaking, organic or mineral nitrogen compound concentrations are usually measured in the vineyard and in grape musts. These indicators facilitate vine cultivation decisions, usually through yield or vigor. During vinification, yeast and bacteria metabolize nitrogen compounds in the musts in order to generate biomass. After fermentation, the microorganisms rerelease a part of this nitrogen as soluble compounds into the wines. Another part remains bound in the lees and can be lost during racking. The must’s natural nitrogen quantities, additional supplements during fermentation, and lees contact management enhance the release of nitrogen compounds to the wines. During ageing these nitrogen compounds – primarily the amino acids – are implicated in the generation of odorous compounds such as heterocycles(1).

STATISTICAL COMPARISON OF GROWTH PARAMETERS OF NINE BIOPROTECTION STRAINS IMPLEMENTED ON ARTIFICIALLY CONTAMINATED SYNTHETIC MUST

In recent years, consumer demand for products without chemical additives increased, becoming a priority for the wine sector. SO₂ is widely used for its multiple properties including antiseptics, antioxidants and antioxidasics and the strategy of bioprotection in winemaking represents now an alternative to this chemical additive. In oenology, results have highlighted the interest of bioprotection to limit the development of microorganisms like Hanseniaspora uvarum and thus reduce the doses of sulphite. Indeed, this species is considered because of its acetic acid and methyl butyl acetate production, the latter can cover the varietal character of wines.

REDUCING NITROGEN FERTILIZATION ALTERS PHENOLIC PROFILES OF VITIS VINIFERA L. CV. CABERNET GERNISCHT WINE OF YANTAI, CHINA

Nitrogen (N) fertilizer is important for grape growth and the quality of wine. It is essential to address the mismatch between N application and wine composition. Cabernet Gernischt (Vitis vinifera L.), as one of the main wine-grape cultivars in China, was introduced to Yantai wine region in 1892. This grape cultivar is traditionally used for quality dry red wine with fruit, spices aroma, ruby red and full-bodied wines. In order to regulate vine growth and improve grape and wine quality, Cabernet Gernischt grapevines were subjected to decreased levels of N treatments, compared to normal N supply treatment, during grape growing seasons of 2019 and 2020.