terclim by ICS banner
IVES 9 IVES Conference Series 9 EXTRACTIBLE COMPOUNDS FROM MICROAGGLOMERATED CORK STOPPERS

EXTRACTIBLE COMPOUNDS FROM MICROAGGLOMERATED CORK STOPPERS

Abstract

After bottling, the wine continues to evolve during storage. The choice of the stopper is an important factor in this evolution. In addition to the oxygen permeability of the closure, the migration of stopper compounds into the wine can also have an impact on the wine organoleptic properties. Many studies have shown that transfers of volatile compounds from the stoppers into the wine can happen depending on the type of closure used (1). Moreover, when cork-made stoppers are used, the migration of phenolic compounds from the stopper into the wine can also occur (2, 3). However, there are few studies on the migration of polyphenols from agglomerated corks treated with supercritical CO₂. Therefore, the present study aimed to quantify the polyphenols released by microagglomerated cork stoppers in hydroalcoholic solutions in comparison with those extracted from natural cork stoppers. Thus, extractions were performed on eight different batches of natural cork stoppers and eleven of microagglomerated cork stoppers treated with supercritical CO₂. For this, six stoppers from each batch were immersed in 400 mL of 12% ethanol solution at 40°C for 10 days. The nineteen macerates were then analyzed by HPLC-DAD-ESI-QQQ to identify and quantify the extracted polyphenols and suberic acid. The microagglomerated corks released significantly fewer polyphenols (i.e., 25 times less). Regarding suberic acid, no differences were observed between both types of cork stoppers. Then, according to the groups obtained by a hierarchical ascending classification based on polyphenol composition, the macerates were pooled in equal volumes to reconstitute four new macerates of natural and/or microagglomerated cork stoppers. These four samples were then submitted to a panel of thirteen judges to perform a sensory profile with olfacto-ry, taste, and mouthfeel descriptors. The results of this sensory profile showed that microagglomerated stoppers appeared to have the lowest overall impact on the olfactory and gustative perception of the hydroalcoholic solutions.

 

1. Culleré, L., Cacho, J., & Ferreira, V. (2009). Comparative study of the aromatic profile of different kinds of wine cork stoppers. Food chemistry, 112(2), 381-387.
2. Azevedo, J., Fernandes, I., Lopes, P., Roseira, I., Cabral, M., Mateus, N., & Freitas, V. (2014). Migration of phenolic compounds from different cork stoppers to wine model solutions : Antioxidant and biological relevance. European Food Research and Technology, 239(6), 951-960.
3. Reis, S. F., Coelho, E., Evtuguin, D. V., Coimbra, M. A., Lopes, P., Cabral, M., Mateus, N., & Freitas, V. (2020). Migration of Tannins and Pectic Polysaccharides from natural cork stoppers to the hydroalcoholic solution. Journal of Agricultural and Food Chemistry, 68(48), 14230-14242.

DOI:

Publication date: February 9, 2024

Issue: OENO Macrowine 2023

Type: Poster

Authors

Anne-Laure Gancel¹, Michaël Jourdes¹, Alexandre Pons1, 2 and Pierre-Louis Teissedre1*

1. Université de Bordeaux, Bordeaux INP, Bordeaux Sciences Agro, UMR 1366 OENOLOGIE, ISVV, 33140 Villenave d’Ornon
2. Tonnellerie Seguin-Moreau, ZI Merpins, 16103, Cognac, France

Contact the author*

Keywords

wine cork stoppers, polyphenols, suberic acid, sensory analysis

Tags

IVES Conference Series | oeno macrowine 2023 | oeno-macrowine

Citation

Related articles…

EUGENOL AS QUALITY MARKER OF WINES AND SPIRITS FROM HYBRID VINES: IMPACT OF DIFFERENT WINEMAKING AND DISTILLATION PROCESSES

Eugenol, widely spread in various plants notably cloves, basil and bay, was identified too in wines from hybrid grapes without contact with oak wood. This aromatic molecule presents a strong spicy note of clove and also antifongic properties. Eugenol was described as an endogenous compound of Baco blanc, from the grapes to the spirits of Armagnac area. Moreover, this compound is a chemical marker of Baco blanc products quality.
Influences of harvest time and different winemaking processes (settling, use of enzymatic preparations, lees content and stock time before distillation) on Baco blanc wine eugenol contents were explored using a two-levels full factorial Design of Experiments (DoEs).

TOWARDS THE SHELF-LIFE PREDICTION OF OLD CHAMPAGNE VINTAGES DEPENDING ON THE BOTTLE CAPACITY

Today, nearly one billion bottles of different sizes and capacities are aging in Champagne cellars while waiting to be put on the market. Among them, several tens of thousands of prestigious cuvees elaborated prior the 2000s are potentially concerned by prolonged aging on lees. However, when it comes to champagne tasting, dissolved CO₂ is a key compound responsible for the very much sought-after effer-vescence in glasses [1]. Yet, the slow decrease of dissolved CO₂ during prolonged aging of the most prestigious cuvees raises the issue of how long a champagne can age before it becomes unable to form CO₂ bubbles during tasting [2].

EVALUATION OF INDIGENOUS CANADIAN YEAST STRAINS AS WINE STARTER CULTURES ON PILOT SCALE FERMENTATIONS

The interactions between geographical and biotic factors, along with the winemaking process, influence the composition and sensorial characteristics of wine¹. In addition to the primary end products of alcoholic fermentation, many secondary metabolites contribute to wine flavor and aroma and their production depends predominantly on the yeast strain carrying out the fermentation. Commercially available strains of S. cerevisiae help improve the reproducibility and predictability of wine quality. However, most commercial wine strains available on the market have been isolated from Europe, are genetically similar, and may not be the ideal strain to reflect the terroir of Canadian vineyards².

ABOUT THE ROLE PLAYED BY THE DIFFERENT POLYPHENOLS ON OXYGEN CONSUMPTION AND ON THE ACCUMULATION OF ACETALDEHYDE ANDSTRECKER ALDEHYDES DURING WINE OXIDATION

In a previous work1, it was suggested that the different contents in delphinidin and catechin of the grapes were determinant on the O2 consumption and Strecker aldehyde (SAs) accumulation rates. Higher delphinidin seemed to be related to a faster O2 consumption and a smaller SAs accumulation rate, and the opposite was observed regarding catechin.
In the present paper, these observations were fully corroborated by adding synthetic delphinidin to a wine model containing polyphenolic fractions (PFs) extracted from garnacha and synthetic catechin to a wine model containing PF extracted from tempranillo: The delphinin-containing garnacha model consumed O₂ significantly faster and accumulated significantly smaller amounts of SAs than the original garnacha model, and the catechin-containing tempranillo model, consumed O2 significantly slower and accumulated significantly higher amounts of SAs than the original tempranillo model.

FLAVONOID POTENTIAL OF MINORITY RED GRAPE VARIETIES

The alteration in the rainfall pattern and the increase in the temperatures associated to global climate change are already affecting wine production in many viticultural regions all around the world (1). In fact, grapes are nowadays ripening earlier from a technological point of view than in the past, but they are not necessarily mature from a phenolic point of view. Consequently, the wines made from these grapes can be unbalanced or show high alcohol content. Dramatic shifts in viticultural areas are currently being projected for the future (2).