Macrowine 2021
IVES 9 IVES Conference Series 9 Influence of the different cork stoppers and sulfur dose in champagne quality

Influence of the different cork stoppers and sulfur dose in champagne quality

Abstract

As is well known, Champagne is a product of the highest quality recognized in the international market. Champagne is a type of sparkling wine made in the Champagne region (France) using the traditional method of champenoise. Aging in the bottle is the final stage before being consumed, and it is considered a time of maturation in which many chemical and sensory changes occur (1). In addition, the stoppers have a very important influence on the quality of the product during bottle aging (2). Today there are different types of corks with different types of oxygen permeabilities (3). This oxygen transfer rate (OTR) through the cork can cause changes in the color, in the aromatic composition and in the organoleptic sensations of the Champagne, causing a loss of its quality (3, 4). For all these reasons, the main objective of this work is to evaluate the effect of different types of cork stoppers in Champagne with different doses of sulfur (added in bottling) for a year. To carry out the study, five types of corks (C1, C2, C3, C4 and C5) with increasing OTRs values and the control with sheet metal closure (Control), and three different doses of sulfur (0, 10 and 20 mg/L) were used. Of all of them, the basic parameters, color and Cielab coordinates, CO2 pressure, aromatic composition (fermentative, oxidative and reduction aromas), and sensory analysis were analyzed at each of the four sampling points. The analysis times were after bottling (T0) and after 3, 6, 12 months of aging in the bottle (T3, T6, T12). The results showed that the parameter ‘time’ was the main factor in producing differences between the samples, followed by the doses of sulfur and type of cork. In general, the basic parameters of champagne did not show significant differences except for total sulfur content. In general, the color, the CO2 parameters and especially the aromatic composition changed over time, showing the main changes after 12 months in the bottle. The fermentation aromas were decreasing, and the oxidation and reduction aromas were increasing over time. The samples with the highest dose of sulfur (20 mg/L) were less evolved, however they showed greater reductions. In addition, C5 and C3 corks with were the corks that best preserved Champagne in relation to the preservation of fermentative aromas, and in achieving a better balance between oxidation-reduction conditions, after 12 months of aging. However, the C2 was the cork that had the worst preservation of fermentative aromas and the greatest oxidation caused the Champagne. Finally, the sensory analysis on time 12 months corroborated analytics, the best valued Champagne being those closed with C3 and C5 corks, and the worst with C2. Therefore, a good choice about the type of cork and the dose of sulfur in bottling can prolong its optimal moment of consumption in time, while preserving its quality.

DOI:

Publication date: September 14, 2021

Issue: Macrowine 2021

Type: Article

Authors

Ana Maria Mislata 

1. VITEC – Centre Tecnològic del Vi, Ctra. Porrera Km 1, 43730 Falset (Tarragona), Spain 2. Instrumental Sensometry (i-Sens), Department of Analytical Chemistry and Organic  Chemistry, Campus Sescelades, Universitat Rovira i Virgili, Tarragona, 43007, Spain ,Michelle Rodríguez 2; Christophe Loisel 3; Miquel Puxeu 1; Enric Nart 1; Sergi De Lamo 1; Montserrat Mestres 2 and Raúl Ferrer-Gallego 1  1. VITEC – Centre Tecnològic del Vi, Ctra. Porrera Km.1, 43730 Falset (Tarragona), Spain 2. Instrumental Sensometry (i-Sens), Department of Analytical Chemistry and Organic  Chemistry, Campus Sescelades, Universitat Rovira i Virgili, Tarragona, 43007, Spain 3. DIAM Bouchage SAS-Espace Tech Ulrich, 66400 Ceret, France

Contact the author

Keywords

champagne, corks, sulfurous, otr, color, aromatic compounds, sensory analysis

Citation

Related articles…

Effects of organic mulches on the soil environment and yield of grapevine

Farming management practices aiming at conserving soil moisture have been developed in arid and semiarid-areas facing water scarcity problems. Organic mulching is an effective method to manipulate the crop-growing microclimate increasing crop yield by controlling soil temperature, and retaining soil moisture by reducing soil evaporation. In this sense, the effectiveness of different organic mulching materials (straw mulch and grapevine pruning debris) applied within the row of a vineyard was evaluated on the soil and on the vine in a Tempranillo vineyard located in La Rioja (Spain). Organic mulches were compared with a traditional bare soil management technique (based on the use of herbicides to avoid weed incidence). Mulching coverages favourably influenced the soil water retention throughout all the grapevine vegetative cycle. However, the soil-moisture variation was not the same under different mulching materials, being the straw mulch (SM) the one that retained more water in comparison with grapevine pruning debris (GPD) based-cover. The changes of soil moisture in the upper surface layer (0–10 cm) were highly dynamic, probably due to water vapour fluxes across the soil-atmospheric interface. However, both, SM and GPD reduced these fluctuations as compared with bare soils. A similar trend occurred with soil temperature. Both organic mulches altered soil temperature in comparison with bare soil by reducing soil temperature in summer and raising it in winter. Moreover, the same buffering effect for the temperature on the covered soil also remains in the deeper layers. To conclude, we could see that organic mulching had a positive impact on soil-moisture storage and soil temperature and the extent of this effect depends on the type of mulching materials. These changes led to higher rates of photosynthesis and stomatal conductivity compared to bare soils, also favouring crop growth and grape yields.

The rootstock, the neglected player in the scion transpiration even during the night

Water is the main limiting factor for yield in viticulture. Improving drought adaptation in viticulture will be an increasingly important issue under climate change. Genetic variability of water deficit responses in grapevine partly results from the rootstocks, making them an attractive and relevant mean to achieve adaptation without changing the scion genotype. The objective of this work was to characterize the rootstock effect on the diurnal regulation of scion transpiration. A large panel of 55 commercial genotypes were grafted onto Cabernet Sauvignon. Three biological repetitions per genotype were analyzed. Potted plants were phenotyped on a greenhouse balance platform capable of assessing real-time water use and maintaining a targeted water deficit intensity. After a 10 days well-watered baseline period, an increasing water deficit was applied for 10 days, followed by a stable water deficit stress for 7 days. Pruning weight, root and aerial dry weight and transpiration were recorded and the experiment was repeated during two years. Transpiration efficiency (ratio between aerial biomass and transpiration) was calculated and δ13C was measured in leaves for the baseline and stable water deficit periods. A large genetic variability was observed within the panel. The rootstock had a significant impact on nocturnal transpiration which was also strongly and positively correlated with maximum daytime transpiration. The correlations with growth and water use efficiency related traits will be discussed. Transpiration data were also related with VPD and soil water content demonstrating the influence of environmental conditions on transpiration. These results highlighted the role of the rootstock in modulating water deficit responses and give insights for rootstock breeding programs aimed at identifying drought tolerant rootstocks. It was also helpful to better define the mechanisms on which the drought tolerance in grapevine rootstocks is based on.

Different soil types and relief influence the quality of Merlot grapes in a relatively small area in the Vipava Valley (Slovenia) in relation to the vine water status

Besides location and microclimatic conditions, soil plays an important role in the quality of grapes and wine. Soil properties influence…

Permanent cover cropping with reduced tillage increased resiliency of wine grape vineyards to climate change

Majority of California’s vineyards rely on supplemental irrigation to overcome abiotic stressors. In the context of climate change, increases in growing season temperatures and crop evapotranspiration pose a risk to adaptation of viticulture to climate change. Vineyard cover crops may mitigate soil erosion and preserve water resources; but there is a lack of information on how they contribute to vineyard resiliency under tillage systems. The aim of this study was to identify the optimum combination of cover crop sand tillage without adversely affecting productivity while preserving plant water status. Two experiments in two contrasting climatic regions were conducted with two cover crops, including a permanent short stature grass (P. bulbosa hybrid), barley (Hordeum spp), and resident vegetation under till vs. no-till systems in a Ruby Cabernet (V. vinifera spp.) (Fresno) and a Cabernet Sauvingon (Napa) vineyard. Results indicated that permanent grass under no-till preserved plant available water until E-L stage 17. Consequently, net carbon assimilation of the permanent grass under no-till system was enhanced compared to those with barley and resident vegetation. On the other hand, the barley under no-till system reduced grapevine net carbon assimilation during berry ripening that led to lower content of nonstructural carbohydrates in shoots at dormancy. Components of yield and berry composition including flavonoid profile at either site were not adversely affected by factors studied. Switching to a permanent cover crop under a no-till system also provided a 9% and 3% benefit in cultural practices costs in Fresno and Napa, respectively. The results of this work provides fundamental information to growers in preserving resiliency of vineyard systems in hot and warm climate regions under context of climate change.

Soil, vine, climate change – what is observed – what is expected

To evaluate the current and future impact of climate change on Viticulture requires an integrated view on a complex interacting system within the soil-plant-atmospheric continuum under continuous change. Aside of the globally observed increase in temperature in basically all viticulture regions for at least four decades, we observe several clear trends at the regional level in the ratio of precipitation to potential evapotranspiration. Additionally the recently published 6th assessment report of the IPCC (The physical science basis) shows case-dependent further expected shifts in climate patterns which will have substantial impacts on the way we will conduct viticulture in the decades to come.
Looking beyond climate developments, we observe rising temperatures in the upper soil layers which will have an impact on the distribution of microbial populations, the decay rate of organic matter or the storage capacity for carbon, thus affecting the emission of greenhouse gases (GHGs) and the viscosity of water in the soil-plant pathway, altering the transport of water. If the upper soil layers dry out faster due to less rainfall and/or increased evapotranspiration driven by higher temperatures, the spectral reflection properties of bare soil change and the transport of latent heat into the fruiting zone is increased putting a higher temperature load on the fruit. Interactions between micro-organisms in the rhizosphere and the grapevine root system are poorly understood but respond to environmental factors (such as increased soil temperatures) and the plant material (rootstock for instance), respectively the cultivation system (for example bio-organic versus conventional). This adds to an extremely complex system to manage in terms of increased resilience, adaptation to and even mitigation of climate change. Nevertheless, taken as a whole, effects on the individual expressions of wines with a given origin, seem highly likely to become more apparent.