New acacia gums fractions: how their features affect the foamability of sparkling base wines?

Abstract

When sparkling wine is served, the first attribute perceived is foam1. Bentonite is usually added to wine in order to cause particle flocculation, but this procedure also leads to a drastic loss of foamability2. Acacia gums improve the foamability of some sparkling base wines treated with bentonite3. Acacia gums are already authorized as additives in wine production4. We studied how the addition of new fractions from Acacia gums affected the wines foamability. Our work deepens the relationship between wine foamability and gums fractions properties. Eight sparkling base wines were elaborated by the traditional white winemaking method. Three of them were elaborated in three different regions from Spain: Malaga using Moscatel grapes as well as Saragossa and Tarragona (TA), both using Macabeo grapes. The other five base wines were elaborated in the French region of Champagne using Chardonnay (4) and Pinot noir (1) grapes. They were treated with bentonite, stirred and filtered. Acacia senegal (Asen) and Acacia seyal (Asey) gums were fractionated by Ion Exchange Chromatography giving two high (F1sen and F1sey) and two low (F2sen and F2sey) molar mass fractions. Fractions and sparkling base wines were deeply characterized. Four Acacia gums fractions were separately added to wines (300 mg·L-1), resulting in “supplemented CO-wines”. Based on shaking test, wine was vigorously hand-shaken in closed tubes. The foam height at 5 and every 10 seconds during 90 seconds was measured (all in triplicate). The maximum foam height was improved in 11 out of the 16 supplementations (69%) with F1 fractions, which were the fractions with high protein amount and high molar mass. F1sey and mainly F1sen showed a positive effect improving the foamability in Spanish wines. F1 fractions also increased foamability of French wines, but in a more inefficient and irregular pattern. Moreover, the differentials of foam height (ΔFH) between “supplemented CO-wines” and CO-wines enhanced significantly in all the studied wines at several moments after supplementations with F1 fractions. F2 fractions gave enhancing effect only sporadically. Adding F1sen and F1sey, the foam height showed positive Pearson correlations with, respectively, (i) polysaccharides rich in arabinose and galactose percentage and (ii) the number average molar mass of polysaccharides. But after F1 supplementations, the mannoproteins percentage in base wines affected negatively their foamability. The Proteins %, the hydrophobic score, the volumetric properties, the molar masses, the high molar mass ranges and the content of several amino acids of gums fractions affected positively the foamability in different wines, whereas it was negatively affected by the sugars %.Concluding, sparkling base wine foamabilities strongly depend on the wine and the gum fraction addition, but also on their relationship.

DOI:

Publication date: September 15, 2021

Issue: Macrowine 2021

Type: Article

Authors

Rafael Apolinar-Valiente, Thomas Salmo, Pascale Williams,  Michaël Nigen, Christian Sanchez, Thierry Doco,  Richard Marchal.

UMR-1208/IATE, Montpellier SupAgro, France.LOCA, Université de Reims, France. UMR-1083/SPO, INRAE-Montpellier, France. UMR-1208/IATE, Université Montpellier, France. UMR-1208/IATE, Université Montpellier, France. UMR-1083/SPO, INRAE-Montpellier, France. LVBE, Université de Haute-Alsace, Colmar, France.

Contact the author

Keywords

sparkling base wine; foam; acacia gums; ion exchange chromatography; macromolecules; sec-malls; biochemical properties; structural features

Citation

Related articles…

Drought effect on aromatic and phenolic potential of seven recovered grapevine varieties in Castilla-La Mancha region (Spain)

The effects of climate change are seriously affecting the quality of wine grapes. High temperatures and drought cause imbalances in the chemical composition of grapes. The result is overripe grapes with low acidity and high sugar content, which produce wines with excessive alcohol content, lacking in freshness and not very aromatic. As a consequence, the search of varieties with capacity of produce quality grapes in adverse climate conditions is a good alternative to preserve the sustainability of vineyards. In this work, quality parameters of seven Vitis vinifera L. cultivars (five whites and two reds) recently recovered from extinction and grown under two different hydric regimes (rainfed and irrigated) were analyzed during the 2020 vintage. At harvest time, weight of 100 berries, must physicochemical parameters (brix degree, total acidity, malic acid, pH), and carbon and oxygen isotope ratios (δ13C, δ18O) were determined. Subsequently, varietal aroma potential index (IPAv) and total polyphenol index (TPI) were analyzed. Quality parameters, IPAv and TPI, showed significant differences between varieties and water regimes. Both red varieties, Moribel and Tinto Fragoso, stood out for their high aromatic and phenolic potential, which was higher under rainfed regime. Regarding to white varieties, Montonera del Casar and Jarrosuelto stood out in terms of varietal aroma potential. Montonera del Casar high acidity in its musts and Jarrosuelto showed the highest berry weights.

Effect of multi-level and multi-scale spectral data source on vineyard state assessment

Currently, the main goal of agriculture is to promote the resilience of agricultural systems in a sustainable way through the improvement of use efficiency of farm resources, increasing crop yield and quality under climate change conditions. This last is expected to drastically modify plant growth, with possible negative effects, especially in arid and semi-arid regions of Europe on the viticultural sector. In this context, the monitoring of spatial behavior of grapevine during the growing season represents an opportunity to improve the plant management, winegrowers’ incomes, and to preserve the environmental health, but it has additional costs for the farmer. Nowadays, UAS equipped with a VIS-NIR multispectral camera (blue, green, red, red-edge, and NIR) represents a good and relatively cheap solution to assess plant status spatial information (by means of a limited set of spectral vegetation indices), representing important support in precision agriculture management during the growing season. While differences between UAS-based multispectral imagery and point-based spectroscopy are well discussed in the literature, their impact on plant status estimation by vegetation indices is not completely investigated in depth. The aim of this study was to assess the performance level of UAS-based multispectral (5 bands across 450-800nm spectral region with a spatial resolution of 5cm) imagery, reconstructed high-resolution satellite (Sentinel-2A) multispectral imagery (13 bands across 400-2500 nm with spatial resolution of <2 m) through Convolutional Neural Network (CNN) approach, and point-based field spectroscopy (collecting 600 wavelengths across 400-1000 nm spectral region with a surface footprint of 1-2 cm) in a plant status estimation application, and then, using Bayesian regularization artificial neural network for leaf chlorophyll content (LCC) and plant water status (LWP) prediction. The test site is a Greco vineyard of southern Italy, where detailed and precise records on soil and atmosphere systems, in-vivo plant monitoring of eco-physiological parameters have been conducted.

VineyardFACE: Investigation of a moderate (+20%) increase of ambient CO2 level on berry ripening dynamics and fruit composition

Climate change and rising atmospheric carbon dioxide concentration is a concern for agriculture, including viticulture. Studies on elevated carbon dioxide have already been on grapevines, mainly taking place in greenhouses using potted plants or using field grown vines under higher CO2 enrichment, i.e. >650 ppm. The VineyardFACE, located at Hochschule Geisenheim University, is an open field Free Air CO2 Enrichment (FACE) experimental set-up designed to study the effects of elevated carbon dioxide using field grown vines (Vitis vinifera L. cvs. Riesling and Cabernet Sauvignon). As the carbon dioxide fumigation started in 2014, the long term effects of elevated carbon dioxide treatment can be investigated on berry ripening parameters and fruit metabolic composition.
The present study aims to investigate the effect on fruit composition under a moderate increase (+20%; eCO2) of carbon dioxide concentration, as predicted for 2050 on both Riesling and Cabernet Sauvignon. Berry composition was determined for primary (sugars, organic acids, amino acids) and secondary metabolites (anthocyanins). Special focus was given on monitoring of berry diameter and ripening rates throughout three growing seasons. Compared to previous results of the early adaptative phase of the vines [1], our results show little effect of eCO2 treatment on primary metabolites composition in berries. However, total anthocyanins concentration in berry skin was lower for eCO2 treatment in 2020, although the ratio between anthocyanins derivatives did not differ.
[1] Wohlfahrt Y., Tittmann S., Schmidt D., Rauhut D., Honermeier B., Stoll M. (2020) The effect of elevated CO2 on berry development and bunch structure of Vitis vinifera L. cvs. Riesling and Cabernet Sauvignon. Applied Science Basel 10: 2486

‘Cabernet Sauvignon’ (Vitis vinifera L.) berry skin flavonol and anthocyanin composition is affected by trellis systems and applied water amounts

Trellis systems are selected in wine grape vineyards to mainly maximize vineyard yield and maintain berry quality. This study was conducted in 2020 and 2021 to evaluate six commonly utilized trellis systems including a vertical shoot positioning (VSP), two relaxed VSPs (VSP60 and VSP80), a single high wire (SH), a high quadrilateral (HQ), and a guyot (GY), combined with three levels of irrigation regimes based on different crop evapotranspiration (ETc) replacements, including a 25% ETc, 50% ETc, and 100% ETc. The results indicated SH yielded the most fruits and accumulated the most total soluble solids (TSS) at harvest in 2020, however, it showed the lowest TSS in the second season. In 2020, SH and HQ showed higher concentrations in most of the anthocyanin derivatives compared to the VSPs. Similar comparisons were noticed in 2021 as well. SH and HQ also accumulated more flavonols in both years compared to other trellis systems. Overall, this study provides information on the efficacy of trellis systems on grapevine yield and berry flavonoid accumulation in a currently warming climate.

Soil quality in Beaujolais vineyard. Importance of pedology and cultural practices

A pedological study was carried out from 2009 to 2017 in Beaujolais vineyard, to improve physical and chemical knowledge of soils. It was completed in 2016 and 2017 by the current study, dealing with microbial aspects, in order to build a reference frame for improved advice in soil management. Microbial biomass was measured on representative plots of the six most common soil types identified in Beaujolais and, for each soil type, on plots with different levels of the main impacting parameters: total organic carbon, pH, cation exchange capacity, extractable copper. A total of 59 soil samples were collected. Confirming the results of various trials carried out in Beaujolais over the past 20 years, the results of the present study showed that the soils were still alive, but exhibited a large variability of biological parameters, which appeared dependant on both pedological and anthropic factors. Therefore, a good interpretation of biological parameters and advice for vine growers must rely on a pedologically-based referential with differentiated main driving factors. For example, the control of pH is of primary importance in granitic soils and in no way organic matter addition can improve soil quality if pH is too low. Conversely, in calcareous soils, biological parameters are more directly affected by direct or indirect (cover crops for example) inputs of organic matter. The use of biological parameters, such as microbial biomass, is of great potential value to improve advice on agro-viticultural practices (soil management, fertilization, liming, etc.), basis of a sustainable wine production on fragile soils.