IVAS 2022 banner
IVES 9 IVES Conference Series 9 IVAS 9 IVAS 2022 9 Targeted and untargeted 1H-NMR analysis for sparkling wine’s authenticity

Targeted and untargeted 1H-NMR analysis for sparkling wine’s authenticity

Abstract

Studies on wineomics (wine’s metabolome) have increased considerably over the last two decades. Wine results from many environmental, human and biological factors leading to a specific metabolome for each terroir. NMR metabolomics is a particularly effective tool for studying the metabolome since it allows the rapid and simultaneous detection of major compounds from several chemical families.1 Quantitative NMR has already proven its effectiveness in monitoring the authenticity of still wines.2 In this study, we wanted to know if these approaches could be effective to guarantee sparkling wine authenticity.More than 100 French sparkling wines from different regions (i.e. Champagne, Crémant de Bordeaux, Crémant d’Alsace and Crémant de Bourgogne) were analysed by targeted and untargeted 1H-NMR approaches. The collected data were statistically processed by principal component analysis (PCA), partial least squares discriminant analysis (PLS-DA) and partial orthogonal least squares discriminant analysis (OPLS-DA). Cross permutation tests and ANOVAs were performed to validate the results.Our results show that 1H-NMR metabolomics discriminates between protected designations of origin. Targeted and untargeted approaches made it possible to establish a profile for each appellation and to determine the chemical compounds significantly involved in the discrimination. Untargeted analysis allows discriminating champagne label of quality.  These analyses highlighted notions of traceability and quality to discriminate appellations of origin from sparkling wines.

DOI:

Publication date: June 27, 2022

Issue: IVAS 2022

Type: Poster

Authors

Le Mao Ines1, Da Costa Gregory1, Bautista Charlyne1 and Richard Tristan1

1UMR 1366, Univ. Bordeaux, INRAE, Bordeaux INP, Bordeaux Science Agro, OENO, ISVV

Contact the author

Keywords

NMR, metabolomics, sparkling wines

 

Tags

IVAS 2022 | IVES Conference Series

Citation

Related articles…

Regional impact on rootstock/scion mediated methoxypyrazine accumulation in rachis

Aim: To investigate the impact of Geographical Indications (GI) of South Australia on the rootstock/scion-mediated methoxypyrazine accumulation within the rachis of Shiraz and Cabernet Sauvignon. 

CHARACTERIZATION AND ANTIBACTERIAL ACTIVITY OF A POLYPHENOLIC EXTRACT OBTAINED BY GREEN SUPERCRITICAL CO₂ EXTRACTION FROM RED GRAPE POMACE

Upgrading wine industry solid wastes is considered as one of the main strategies to support the circular economy. Red grape pomaces constitute a rich source of polyphenols, which have been shown to possess antioxidant properties and to provide benefits for human and animal health. The objective of this work was to obtain and characterise polyphenolic extracts from red grape pomaces via green supercritical CO₂ extraction using ethanol as a co-solvent, and to evaluate their antibacterial activity against susceptible and multidrug-resistant Escherichia coli strains of animal intestinal origin.

Potentiel des sols viticoles et qualité des vins

La qualité des vins dépend de différents facteurs et procédés, notamment de la nature des terrains viticoles. Dans ce travail, nous avons cherché à établir les liens entre descripteurs pédologiques des parcelles et descripteurs sensoriels des vins. Sur la base de Classifications Ascendantes Hiérarchiques (CAH) et d’Analyses en Composante Principale (ACP), il a été possible d’établir des liens entre la nature des parcelles (sableuse, argileuse, sablo-graveuleuse) et certains descripteurs sensoriels des vins (chaleur, astringence, fruit noir) et plus globalement avec le type de vins élaborés.

Evaluation of climate change impacts at the Portuguese Dão terroir over the last decades: observed effects on bioclimatic indices and grapevine phenology

In the last decades the growers of the Portuguese Dão winegrowing region (center of Portugal) are experiencing changes in climate that are influencing either grape phenology berry health and ripening. Aiming to study the relationships between climate indices (CI), seasonal weather and grapevine phenology, in this work long-term climate and phenological data collected at the experimental vineyard of the Portuguese Dão research centre between 1958 and 2019 (61 years) for the red variety Touriga Nacional, was analyzed. The trends over time for the classical temperature-based indices (Growing Season Temperature – GST -, Growing Degree Days – GDD, Huglin Index – HI and Cool Night Index – CI) presented a significantly positive slope while the Dryness Index (DI) showed a negative trend over the last 61 years. Regarding grapevine phenology, an average advance of 4.5 days per decade in the harvest day was observed throughout the last 61 years. Consequently, the weather conditions during the ripening period have changed, showing an increasing trend over time in the average temperature (higher magnitude in the maximum than in the minimum temperature) and a decrease in the accumulated rainfall. A regression analysis showed that ~50% of harvest date variability over years was explained by the temperature-based indices variability. These observed effects of climate change on bioclimatic indices and corresponding anticipation of harvest date can still be considered advantageous for the Dão terroir as it allows to achieve an optimal berry ripening before the common equinox rains and, therefore, avoid the potential negative impacts of the rainfall on berry health and composition.

Sardinia terroir and Cannonau: a zoning approach to discover an ancient tradition

Cannonau variety is historically grown in a large Sardinia area (Jerzu district) and the vineyards are planted both in the plane and in the sloped hills reaching also 650 m of altitude a.s.l. Thus, in order to discover how climate, soil diversity and growing traditions could account for differences in grape and wine quality, this trial was carried out.