terclim by ICS banner
IVES 9 IVES Conference Series 9 IMPACT OF CLIMATIC CONDITIONS ON THE SEASONING QUALITY OF OAK WOOD FOR OENOLOGICAL USE (QUERCUS PETRAEA)

IMPACT OF CLIMATIC CONDITIONS ON THE SEASONING QUALITY OF OAK WOOD FOR OENOLOGICAL USE (QUERCUS PETRAEA)

Abstract

For coopers, seasoning and toasting are considered crucial steps in barrel making during which the oak wood develops specific organoleptic properties. Seasoning, carried out in the open air, allows reducing the moisture content of the staves to between 14 and 18% (compared to 70 to 90% after splitting) while modulating the intrinsic composition of the oak wood. Toasting consists of applying different degrees of heat to a barrel for a specific period of time. As the temperature increases, oak wood produces a wide range of chemical compounds through thermal degradation of its intrinsic composition. Many studies have been conducted to identify the key aroma compounds in oak wood, and in a recent work we re-ported the identification of two new unsaturated aldehydes responsible for the “puff pastry” and “me-tallic” nuances present in toasted oak wood aroma: (2E,4E,6Z)-nonatrienal (I) and trans-4,5-epoxy-(E)-2- decenal (II).1 In foods, these aldehydes are derived from the oxidative degradation of linolenic and linoleic acids, respectively. This degradation is promoted by heat, light and metal ions. However, no data are available on the presence of fatty acids in oak wood for oenological use (Quercus petraea). In this context, this work aimed to study the distribution of fatty acids in oak wood by focusing on the seaso-ning process taking into account the impact of climatic conditions. To do so, we studied in parallel the evolution and distribution of unsaturated aldehydes and fatty acids in seven oak wood staves during the seasoning process (0, 12, 18 and 36 months) depending on the location (Merpins, Châlon-en-Cham-pagne and Beaumes-de-Venise). They were selected for their climatic diversity (average temperature and rainfall). Based on this experimental protocol, 84 samples were analyzed. The study of unsaturated aldehydes was carried out by GC-NCI-MS (NH₃) analysis, while the study of fatty acids required the de-velopment of a quantification method by GC-TOF MS analysis after liquid-liquid extraction and deriva-tisation. The results show a significant impact of climatic conditions on the distribution of unsaturated aldehydes and fatty acids. For example, the highest levels of unsaturated aldehydes (1.5 ng/g wood (I) and 13.2 ng/g wood (II)) were detected in oak wood seasoned in Merpins and Beaumes-de-Venise (southern France) compared to that seasoned in Châlon-en-Champagne (northern France). Conversely, linolenic acid was detected at a higher level in seasoned oak wood in Châlon-en-Champagne (9.5 µg/g wood). It is likely that “warm” climates lead to a degradation of fatty acids in favor of the formation of unsaturated aldehydes. These new results underline the potential effect of global warming on the quality and sensory identity of oak wood and barrels. To go further, these samples were also toasted. The impact on the aroma of red wine will be discussed.

 

1. Courregelongue, M., Shinkaruk, S., Prida, A., Darriet, P., & Pons, A. (2022). Identification and Distribution of New Impact Aldehydes in Toasted Oak Wood ( Quercus petraea ). Journal of Agricultural and Food Chemistry, acs.jafc.2c01828. https://doi.org/10.1021/acs.jafc.2c01828

DOI:

Publication date: February 9, 2024

Issue: OENO Macrowine 2023

Type: Article

Authors

Marie Courregelongue 1,2,3, Andrei Prida 3, Alexandre Pons 1,2,3

1. Univ. Bordeaux, Bordeaux INP, INRAE, OENO, UMR 1366, ISVV, F-33140 Villenave d’Ornon, France
2. Bordeaux Sciences Agro, F-33170 Gradignan, France
3. Seguin Moreau Cooperage, ZI Merpins, F-16103 Cognac, France

Contact the author*

Keywords

oak wood, fatty acids, unsaturated aldehydes, climate change

Tags

IVES Conference Series | oeno macrowine 2023 | oeno-macrowine

Citation

Related articles…

WINE FERMENTATION METABOLITES PRODUCED BY TWO TORULASPORA DELBRUECKII STRAINS ISOLATED FROM OKANAGAN VALLEY, BC, CANADA VINEYARDS

Wine aroma is influenced by various factors, from agricultural practices in the vineyard to the enological choices made by winemakers throughout the vinification process. Spontaneous fermentations have a characteristically deeper complexity of aromas when compared to fermentations that have been inoculated with Saccharomyces (S.) cerevisiae because of the diversity of microflora naturally present on grape skins. Non-Saccharomyces yeast are being extensively studied for their ability to positively contribute to wine aroma and flavour. These yeasts are known to liberate more bound volatile compounds present in grape must than S. cerevisiae through the enzymatic action of β-glucosidases and β-lyases1.

AGEING BOTTLED WINES SUBMERGED IN SEA: DOES IT IMPACT WINE COMPOSITION?

Aging wines is a common practice in oenology, which in recent years has undergone some innovations. Currently, we are witnessing the practice of aging bottled wine in depth, immersed in the sea or in reservoirs, for variable periods of time, but so far, little is known about the impact of aging in depth on the physicochemical properties, of wines.
The objective of this work was to evaluate the impact of this practice on the physicochemical characteristics, in particular to verify changes in the volatile composition of wines bottled and subsequently immersed in depth. A red wine from Cabernet Sauvignon was bottled and a set of bottles were submerged from July to February (2020), another set of bottles were submerged from February to September (2020) and another set was kept in the wine cellar. Bottles from each set were analyzed (in triplicate) in July 2021.

‘TROPICAL’ POLYFUNCTIONAL THIOLS AND THEIR ROLE IN AUSTRALIAN RED WINES

Following anecdotal evidence of unwanted ‘tropical’ character in red wines resulting from vineyard interventions and a subsequent yeast trial observing higher ‘red fruit’ character correlated with higher thiol concentrations, the role of polyfunctional thiols in commercial Australian red wines was investigated.
First, trials into the known tropical thiol modulation technique of foliar applications of sulfur and urea were conducted in parallel on Chardonnay and Shiraz.1 The Chardonnay wines showed expected results with elevated concentrations of 3-sulfanylhexanol (3-SH) and 3-sulfanylhexyl acetate (3-SHA), whereas the Shiraz wines lacked 3-SHA. Furthermore, the Shiraz wines were described as ‘drain’ (known as ‘reductive’ aroma character) during sensory evaluation although they did not contain thiols traditionally associated with ‘reductive’ thiols (H2S, methanethiol etc.).

VOLATILE COMPOSITION OF WINES USING A GC/TOFMS: HS-SPME VS MICRO LLE AS SAMPLE PREPARATION METHODOLOGY

Wine aroma analysis can be done by sensorial or instrumental analysis, the latter involving several me-thodologies based on olfactometric detection, electronic noses or gas chromatography. Gas Chromatography has been widely used for the study of the volatile composition of wines and depending on the detection system coupled to the chromatographic system, quantification and identification of individual compounds can be achieved.

HOW DOES ULTRASOUND TREATMENT AFFECT THE AGEING PROFILE OF AN ITALIAN RED WINE?

Many wine styles require moderate or extended ageing to ensure optimal consumer experience. However, few consumers have the interest or ability to age wine themselves, and holding wine in optimal conditions for extended periods is expensive for producers. A study was conducted on the use of ul-trasound energy on wine, with particular reference to its impact on sensory and chemical profiles. The OIV has authorised the use of ultrasound for processing crushed grapes (must) in Resolution OENO 616-2019, but not yet for finished wine1,2.