terclim by ICS banner
IVES 9 IVES Conference Series 9 IMPACT OF CLIMATIC CONDITIONS ON THE SEASONING QUALITY OF OAK WOOD FOR OENOLOGICAL USE (QUERCUS PETRAEA)

IMPACT OF CLIMATIC CONDITIONS ON THE SEASONING QUALITY OF OAK WOOD FOR OENOLOGICAL USE (QUERCUS PETRAEA)

Abstract

For coopers, seasoning and toasting are considered crucial steps in barrel making during which the oak wood develops specific organoleptic properties. Seasoning, carried out in the open air, allows reducing the moisture content of the staves to between 14 and 18% (compared to 70 to 90% after splitting) while modulating the intrinsic composition of the oak wood. Toasting consists of applying different degrees of heat to a barrel for a specific period of time. As the temperature increases, oak wood produces a wide range of chemical compounds through thermal degradation of its intrinsic composition. Many studies have been conducted to identify the key aroma compounds in oak wood, and in a recent work we re-ported the identification of two new unsaturated aldehydes responsible for the “puff pastry” and “me-tallic” nuances present in toasted oak wood aroma: (2E,4E,6Z)-nonatrienal (I) and trans-4,5-epoxy-(E)-2- decenal (II).1 In foods, these aldehydes are derived from the oxidative degradation of linolenic and linoleic acids, respectively. This degradation is promoted by heat, light and metal ions. However, no data are available on the presence of fatty acids in oak wood for oenological use (Quercus petraea). In this context, this work aimed to study the distribution of fatty acids in oak wood by focusing on the seaso-ning process taking into account the impact of climatic conditions. To do so, we studied in parallel the evolution and distribution of unsaturated aldehydes and fatty acids in seven oak wood staves during the seasoning process (0, 12, 18 and 36 months) depending on the location (Merpins, Châlon-en-Cham-pagne and Beaumes-de-Venise). They were selected for their climatic diversity (average temperature and rainfall). Based on this experimental protocol, 84 samples were analyzed. The study of unsaturated aldehydes was carried out by GC-NCI-MS (NH₃) analysis, while the study of fatty acids required the de-velopment of a quantification method by GC-TOF MS analysis after liquid-liquid extraction and deriva-tisation. The results show a significant impact of climatic conditions on the distribution of unsaturated aldehydes and fatty acids. For example, the highest levels of unsaturated aldehydes (1.5 ng/g wood (I) and 13.2 ng/g wood (II)) were detected in oak wood seasoned in Merpins and Beaumes-de-Venise (southern France) compared to that seasoned in Châlon-en-Champagne (northern France). Conversely, linolenic acid was detected at a higher level in seasoned oak wood in Châlon-en-Champagne (9.5 µg/g wood). It is likely that “warm” climates lead to a degradation of fatty acids in favor of the formation of unsaturated aldehydes. These new results underline the potential effect of global warming on the quality and sensory identity of oak wood and barrels. To go further, these samples were also toasted. The impact on the aroma of red wine will be discussed.

 

1. Courregelongue, M., Shinkaruk, S., Prida, A., Darriet, P., & Pons, A. (2022). Identification and Distribution of New Impact Aldehydes in Toasted Oak Wood ( Quercus petraea ). Journal of Agricultural and Food Chemistry, acs.jafc.2c01828. https://doi.org/10.1021/acs.jafc.2c01828

DOI:

Publication date: February 9, 2024

Issue: OENO Macrowine 2023

Type: Article

Authors

Marie Courregelongue 1,2,3, Andrei Prida 3, Alexandre Pons 1,2,3

1. Univ. Bordeaux, Bordeaux INP, INRAE, OENO, UMR 1366, ISVV, F-33140 Villenave d’Ornon, France
2. Bordeaux Sciences Agro, F-33170 Gradignan, France
3. Seguin Moreau Cooperage, ZI Merpins, F-16103 Cognac, France

Contact the author*

Keywords

oak wood, fatty acids, unsaturated aldehydes, climate change

Tags

IVES Conference Series | oeno macrowine 2023 | oeno-macrowine

Citation

Related articles…

EXPLORING THE INFLUENCE OF S. CEREVISIAE MANNOPROTEINS ON WINE ASTRINGENCY AND THE IMPACT OF THEIR POLYSACCHARIDE STRUCTURE

Mannoproteins (MPs) are proteoglycans from the outmost layer of yeast cell walls released into wine during alcoholic fermentation and ageing on lees processes. The use of commercial preparations of mannoproteins as additives to improve wine stability with regards to the crystallization of tartaric salts and to prevent protein haze in the case of white and rosé wines is authorized by the OIV.
Regarding red wines and polyphenols, mannoproteins are described as able to improve their colloidal stability and modulate the astringent effect of condensed tannins. The latter interact with salivary proteins forming insoluble aggregates that cause a loss of lubrication in the mouth and promote a drying and puckering sensation. However, neither the interaction mechanisms involved in mannoproteins capacity to impact astringency nor the structure-function relationships related to this property are fully understood.

DETERMINATION OF FREE AMINO ACIDS, AMINO ACID POTENTIAL AND PROTEASE ACTIVITY IN THE LEES AND STILL WINES OF CHAMPAGNE

Prior to winemaking, organic or mineral nitrogen compound concentrations are usually measured in the vineyard and in grape musts. These indicators facilitate vine cultivation decisions, usually through yield or vigor. During vinification, yeast and bacteria metabolize nitrogen compounds in the musts in order to generate biomass. After fermentation, the microorganisms rerelease a part of this nitrogen as soluble compounds into the wines. Another part remains bound in the lees and can be lost during racking. The must’s natural nitrogen quantities, additional supplements during fermentation, and lees contact management enhance the release of nitrogen compounds to the wines. During ageing these nitrogen compounds – primarily the amino acids – are implicated in the generation of odorous compounds such as heterocycles(1).

SENSORY DEFINITION OF A TECHNICAL UNAVOIDABLE TRANSFER OF AROMA COMPOUNDS VIA SEALING IN A BOTTLING LINE IN ORDER TO PREVENT PROSECUTION DUE TO FRAUDULENT AROMATIZATION OF A SUBSEQUENTLY FILLED WINE

In 2020, 12% of all bottled German wines were aromatized, which may increase further due to rising popularity of dealcoholized wines. As sealing polymers of a bottling line absorb aroma compounds and may release them into regular wines in the next filling¹, this unintentional carry-over bears the risk to violate the legal ban of any aromatization of regular wine. However, following EU legislation, German food control authorities accept a technical unavoidable transfer of aroma compounds, if this is of no sensory significance.

PERCEPTUAL INTERACTIONS PHENOMENA INVOLVING VARIOUS VOLATILE COMPOUND FAMILIES LINKED TO SOME FRUITY NOTES IN BORDEAUX RED WINES

Fruity notes play a key role in the consumer’s appreciation of Bordeaux red wines. If literature provides a lot of knowledge about the nature of volatile compounds involved in this fruity expression, the sensory phenomena involving these compounds in mixture still need to be explored. Considering previous sensory works about the impact of esters and some overripening compounds, the goal of this work was to study the implication of perceptual interactions involving red wine odorant compounds of diverse origins and described as potentially affecting fruity aromatic expression.

INVESTIGATION INTO MOUSY OFF-FLAVOR IN WINE USING GAS CHROMATOGRAPHY-MASS SPECTROMETRY WITH STIR BAR SORPTIVE EXTRACTION

Mousy off-flavor is one of the defects of microbial origin in wine. It is described as a particularly unpleasant defect reminiscent of rodent urine (a “dirty mouse cage”), and grilled foods such as popcorn, rice, crackers, and bread crust. Prior to the 2010s, mousiness was very uncommon but it has been becoming more frequent in recent years. It is often associated with an increase in pH as well as certain oenological practices, which tend to significantly decrease the use of sulfur dioxide.